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2, 25°C) for [6,6]-closed fullerene[60] structures, (a) Smith III, A. B.; Strongin, R. M.; Brard, L.; Furst, G. T.; Romanow, W. J. J. Am. Chem. Soc. 1993, 115, 5829.
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+, where M is the MW of the fullerene, X is a tagging crown ether species (m/e=401) and K is a potassium ion captured by crown ether (m/e=39). This tagging technique has been proven to be very useful in the study of fullerene chemistry: (a) Wilson, S. R.; Wu, Y. J. Am. Soc. Mass Spectrom. 1993, 4, 596.
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85031216733
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note
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HPLC - Trident-Tri-DNP "Buckyclutcher I" (Regis Chemical Company). Flow rate: 1 ml/mm, detection: 354 nm. Eluent and retention time: 4d, toluene, 5.53 and 6.12 mm; 4e, toluene/hexane (7/3), 6.36 and 7.05 min; 4f, toluene/hexane (7/3), 6.33 min. 4g, toluene/hexane (1/1), 12.14 and 12.84 min.
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33751385566
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(a)Wilson, S.R.; Wu, Y.; Kaprinidis, N.A.; Schuster, D.I.; Welch, C.J. J. Org. Chem, 1993, 58, 6548.
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Welch, C.J.5
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85031227791
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in press
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(b)Wilson, S.R.; Lu, Q.; Cao, J.; Wu, Y.; Welch, C.J.; Schuster, DI. Tetrahedron, in press.
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Tetrahedron
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Wilson, S.R.1
Lu, Q.2
Cao, J.3
Wu, Y.4
Welch, C.J.5
Schuster, D.I.6
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