Synthesis and Characterisation of the methanofullerenes, C60(CHCN) and C60(CBr2)

Tetrahedron Letters

Volumn 37, Issue 7, 1996, Pages 1085-1086

  Benito, Ana M ^a   Darwish, Adam D ^a   Kroto, Harold W ^a   Meidine, Mohammed F ^a   Taylor, Roger ^a   Walton, David R M ^a  

^a UNIVERSITY OF SUSSEX   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

FULLERENE DERIVATIVE; POLYCYCLIC HYDROCARBON;

ARTICLE; DRUG SYNTHESIS; REACTION ANALYSIS; TECHNIQUE;

EID: 0030061566     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(95)02256-2     Document Type: Article

References (13)

1. Taylor, R.; Walton, D.R.M. Nature 1993, 363, 685-693.
2. Hirsch, A. The Chemistry of the Fullerenes; Georg Thieme Verlag: Stuttgart, 1994.
3. Suzuki, T; Li, Q.; Khemani, K.C.; Wudl, F.; Almarsson, Ö. Science 1991, 254, 1186-1188.
4. Diederich, F.; Isacs, I;. Philp, D. Chemical Society Reviews 1994, 23, 243-255.
5. Bingel, C. Chem.Ber. 1993, 126, 1957-1959.
6. Hirsch, A.; Lamparth, I.; Karfunkel, H.R. Angew.Chem. Int. Ed. Engl. 1994, 33, 437-438.
7. Suzuki, T.; Li Q.; Khemani, K.C.; Wudl, F. J. Am. Chem. Soc. 1992, 114, 7301-7302.
8. Ahlbrecht, H.; Pfaff, K. Synthesis 1978, 897.
9. 13C n.m.r. (125.76 MHz) signals in the fullerene region. δ 145.45 (2), 145.37 (2), 145.36 (2), 144.89 (1), 144.87 (2), 144.75 (2), 144.64 (2), 144.36 (1), 143.78 (2), 143.44 (2), 143.24 (2), 142.88 (1), 142.33 (2), 142.18 (2), 141.24 (2), 139.25 (2).
10. 13C n.m.r. (125.76 MHz) signals in the fullerene region. δ 146 (2), 145.59 (2), 145.51 (2), 145.47 (2), 145.44 (2), 145.17 (2), 145.09 (2), 145.08 (2), 145.07 (2), 145.05 (2), 144.92 (2), 144.81 (2), 144.56 (2), 144.55 (1), 144.42 (1), 143.98 (2), 143.89 (2), 143.30 (2), 143.17 (4), 143.10 (2), 143.09 (1), 143.05 (1), 142.53 (2), 142.26 (2), 142.22 (2), 142.15 (2), 141.43 (2), 141.40 (2), 139.06 (2), 137.40 (2). The signal at 143.17 ppm could not be resolved.
11. Suzuki, T.; Li, Q.; Khemani, K.C.; Wudl, F. J. Am. Chem. Soc. 1992, 114, 7300-7301.
12. Anderson, H.L.; Faust, R.; Rubin, Y.; Diederich, F. Angew. Chem. Int. Ed. Engl. 1994, 33, 1366-1368 .
13. Tsuda, M.; Ishida, T.; Nogami, T.; Kurono, S.; Ohashi, M. Tetrahedron Letters 1993, 34, 6911-6912.