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Volumn 37, Issue 7, 1996, Pages 1003-1006

Solid support synthesis of highly functionalized pyrazoles and isoxazoles; scaffolds for molecular diversity

Author keywords

[No Author keywords available]

Indexed keywords

ISOXAZOLE DERIVATIVE; PYRAZOLE DERIVATIVE;

EID: 0030061466     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(95)02370-4     Document Type: Article
Times cited : (80)

References (15)
  • 3
  • 5
    • 85030190100 scopus 로고    scopus 로고
    • note
    • 3CN/0.1% TFA over 30 min, 1 ml/min. A. part of the eluate (split 1:25) was introduced into a Quattro-BQ mass spectrometer (VG Biotech, Altrincham, England), operated at a source temperature of 60°C and a cone voltage of 50 V, via an electrospray interface (El). The mass range from 100 to 800 Dalton was scanned in 4 seconds.
  • 8
    • 0014772602 scopus 로고
    • 2-linker group was acylated with 0.3M-solution of acetyl carboxylic acid (3eq) at RT (preactivation 40min with 3.3eq DICD and 3.3eq HOBt) until the Kaiser test (Kaiser, E. et al. Anal. Biochem. 1970, 34, 595) was negative.
    • (1970) Anal. Biochem. , vol.34 , pp. 595
    • Kaiser, E.1
  • 11
    • 85030190140 scopus 로고    scopus 로고
    • note
    • 2O, DMA, DMSO, and i-PrOH), and dried under reduced pressure.
  • 12
    • 85030193515 scopus 로고    scopus 로고
    • note
    • 2 and THF.
  • 14
    • 85030188483 scopus 로고    scopus 로고
    • note
    • 5.
  • 15
    • 85030191353 scopus 로고    scopus 로고
    • note
    • +).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.