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27
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13344254905
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note
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Compounds 5, 8, and 12 formed stable solvates with water, DMF, and DMSO and were difficult to obtain in the free form. Attempts to generate accurate C, H, N analyses failed, perhaps because of this solvation phenomenon.
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28
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13344253413
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note
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Lowering the pH to 4 or below causes relatively rapid decarboxylation and generates a mixture of mono- and didecarboxylated products.
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