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Volumn 26, Issue 3, 1996, Pages 535-542

Application of microwave irradiation techniques for the Knoevenagel condensation

Author keywords

[No Author keywords available]

Indexed keywords

ACRYLIC ACID DERIVATIVE; MALONIC ACID DERIVATIVE;

EID: 0030047465     PISSN: 00397911     EISSN: None     Source Type: Journal    
DOI: 10.1080/00397919608003646     Document Type: Article
Times cited : (37)

References (26)
  • 4
    • 85035156218 scopus 로고    scopus 로고
    • M.S. thesis of N.Y. Shim, 12/1993 (Pohang Univ.)
    • (b) M.S. thesis of N.Y. Shim, 12/1993 (Pohang Univ.)
  • 8
    • 85035156994 scopus 로고    scopus 로고
    • note
    • Procedure of 8 by conventional heating; A solution of 10 mL of dry benzene (distilled from sodium), 2.58g(16,6mmol) of 1-naphthaldehyde, 2.90g(18.1mmol) of diethyl malonate, 2mL of piperidine and molecular sieves were stirred (with reflux condenser) at 55°C for 24hr. The solution was cooled to room temperature and water was added. The mixture was extracted with ethyl acetate. The organic phases were dried with magnesium sulfate.The solution was filtered and concentrated under vacuum. The mixture was purified by silicagel chromatography to give 2.2g(7.38mmole, 44.7%) of 8.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.