메뉴 건너뛰기




Volumn 52, Issue 5, 1996, Pages 1643-1650

Lithiomethyl ethyl ether from chloromethyl ethyl ether via a DTBB-catalysed lithiation

Author keywords

[No Author keywords available]

Indexed keywords

ETHER DERIVATIVE;

EID: 0030031289     PISSN: 00404020     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4020(95)00993-0     Document Type: Article
Times cited : (22)

References (43)
  • 1
    • 0004111873 scopus 로고
    • Hase, T. A. Ed.; John Wiley & Sons: New York
    • For a review, see: Saavedra, J. E. In Umpoled Synthons, Hase, T. A. Ed.; John Wiley & Sons: New York, 1987; pp. 101-143.
    • (1987) Umpoled Synthons , pp. 101-143
    • Saavedra, J.E.1
  • 4
    • 5044246846 scopus 로고
    • See, for instance: (a) Still, W. C. J. Am. Chem. Soc. 1978, 100, 1481-1487.
    • (1978) J. Am. Chem. Soc. , vol.100 , pp. 1481-1487
    • Still, W.C.1
  • 16
    • 0001166977 scopus 로고
    • For recent reports, see also
    • For a review, see: (a) Cohen, T.; Bhupathy, M. Acc. Chem. Res. 1989, 22, 152-161. For recent reports, see also:
    • (1989) Acc. Chem. Res. , vol.22 , pp. 152-161
    • Cohen, T.1    Bhupathy, M.2
  • 26
    • 85031211863 scopus 로고    scopus 로고
    • note
    • An alternative route consists in the transformation of a chloromethyl ether into the corresponding trichlorostannyl derivative followed by low temperature tin/lithium transmetallation with n-butyllithium (ref 4d).
  • 30
  • 32
    • 0028928103 scopus 로고
    • See also the accompanying paper in this issue, pp. 1797-1810
    • For the last paper on this topic from our laboratory, see: Alonso, E.; Guijarro, D.; Yus, M. Tetrahedron 1995, 51, 2699-2708. See also the accompanying paper in this issue, pp. 1797-1810.
    • (1995) Tetrahedron , vol.51 , pp. 2699-2708
    • Alonso, E.1    Guijarro, D.2    Yus, M.3
  • 33
    • 0028952540 scopus 로고
    • See also the accompanying paper in this issue, pp. 1797-1810
    • For the last paper on this topic from our laboratory, see: Huerta, F.F.; Gómez, C.; Guijarro, A.; Yus. M. Tetrahedron 1995, 51, 3375-3388. See also the accompanying paper in this issue, pp. 1797-1810.
    • (1995) Tetrahedron , vol.51 , pp. 3375-3388
    • Huerta, F.F.1    Gómez, C.2    Guijarro, A.3    Yus, M.4
  • 34
    • 0028838031 scopus 로고
    • See also the accompanying paper in this issue, pp. 1797-1810
    • For the last paper on this topic from our laboratory, see: Guijarro, A.; Yus, M. Tetrahedron 1995, 51, 231-234. See also the accompanying paper in this issue, pp. 1797-1810.
    • (1995) Tetrahedron , vol.51 , pp. 231-234
    • Guijarro, A.1    Yus, M.2
  • 36
    • 85031234791 scopus 로고    scopus 로고
    • note
    • 2SiCl was used as electrophile, it was necessary to keep the temperature between -90 and -80°C for 30 min before the hydrolysis in order to obtain the best results.
  • 37
    • 85031234637 scopus 로고    scopus 로고
    • note
    • (a) For benzonitrile the temperature was allowed to rise to -60°C for 3 h. (b) In the case of benzonitrile acidification with acetic acid is necessary prior the extraction in order to avoid undesirable by-products.
  • 43
    • 0027372541 scopus 로고
    • Pau, A.; Boatto, G.; Cerri, R.; Palomba, M.; Nicolai, M.; Sparatore, F.; Varoni, M. V. Farmaco 1993, 48, 1291-1299; Chem. Abstr. 1994, 120, 207908u.
    • (1994) Chem. Abstr. , vol.120


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.