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85031232020
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note
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1
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8
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85031219713
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note
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1H NMR spectrum of the crude product, particularly by the triplet at δ 4.92 , due to the acetal proton.
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9
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0010366704
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85031231473
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note
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1H NMR spectrum of the crude product.
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11
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85031224022
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note
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The configuration was assigned by comparing the chemical shift of the olefinic proton with those of (E)-and (Z)-2 a.
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14
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0004538601
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