Reaction of thianthrene cation radical with alcohols: Isolation and chemistry of 5-cyclohexyloxythianthreniumyl perchlorate

Tetrahedron Letters

Volumn 37, Issue 11, 1996, Pages 1749-1750

  Zhao, Wenyi ^a,b   Shine, Henry J ^a  

^a TEXAS TECH UNIVERSITY   (United States)

^b INSTITUTE OF GEOLOGY AND GEOPHYSICS   (China)

Author keywords

[No Author keywords available]

Indexed keywords

1,4 DITHIANE DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; NUCLEAR MAGNETIC RESONANCE; REACTION ANALYSIS;

EID: 0029986720     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(96)00166-9     Document Type: Article

References (5)

1. Shine, H. J.; Yueh, W. Tetrahedron Letters 1992, 33, 6583.
2. Shine, H. J.; Yueh, W. J. Org. Chem. 1994, 59, 3553.
3. - by other workers, it has exploded twice in this laboratory in the course of many years of usage. It should be prepared in small quantities. We do not recommend storing it or filtering it on sintered glass surfaces.
4. 10% carbowax 20 M on 80-100 mesh chrom WHP, 6 ft × 1/8 in stainless steel for cyclohexene; 10% OV-101 on 80-100 mesh chrom WHP, 4 ft × 1/8 in s.s. for all other products.
5. Khuddus, M. A.; Swern, D. J. Am. Chem. Soc. 1973, 95, 8393.