Detection and quantitation of amphetamine and methamphetamine: Electron impact and chemical ionization with ammonia - Comparative investigation on shimadzu QP 5000 GC-MS system

Journal of Analytical Toxicology

Volumn 20, Issue 4, 1996, Pages 255-261

  Dallakian, P ^a   Budzikiewicz, H ^a   Brzezinka, H ^b  

^a UNIVERSITY OF COLOGNE   (Germany)

^b UNIVERSITY OF BONN   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

AMMONIA; AMPHETAMINE; METHAMPHETAMINE;

ACCURACY; ARTICLE; DRUG DETERMINATION; GAS CHROMATOGRAPHY; HUMAN; MASS SPECTROMETRY; URINALYSIS;

EID: 0029979913     PISSN: 01464760     EISSN: None     Source Type: Journal    
DOI: 10.1093/jat/20.4.255     Document Type: Article

References (18)

1. Y. Yoo, H. Chung, and H. Choi. Urinary methamphetamine concentration following famprofazone administration. J. Anal. Toxicol. 18: 265-68 (1994).
2. H. Gjerde, I. Hasvold, G. Petersen, and A.S. Christophersen. Determination of amphetamine and methamphetamine in blood by derivatization with perfluorooctanoyl chloride and gas chromatography/mass spectrometry. J. Anal. Toxicol. 17: 65-68 (1993).
3. P.B. Dallakian and G.P. Voskerchian. The Drugs of Abuse in Russia. Contributions to Forensic Toxicology. Proceedings of the 31st International Meeting of the International Association of Forensic Toxicologists TIAFT Leipzig '93. Ed. by R. Klaus Mueller, Molina Press, Leipzig 1994, pp 164-70.
4. A. Tracqui, M.H. Ghysel, P. Kintz, and P. Mangin. Ecstasy, Eve, Speed. Les nouveaux stimulants de la vigilance et de l'amour, J. de Médecine Légale Droit Médical 38: 145-50 (1995).
5. A.R.W. Forrest, J.H. Galloway, I.D. Marsh, G.A. Strachan, and J.C. Clark. A fatal overdose with 3,4-methylenedioxyamphetamine derivatives. Forensic Sci. Int. 64: 57-59 (1994).
6. B.A. Goldberger and E.J. Cone. Confirmatory tests for drugs in the workplace by gas chromatography-mass spectrometry. J. Chromatogr. 674: 73-86 (1994).
7. R.M.E. Franssen, L.M.L. Stolk, W. van den Brand, and B.J. Smit. Analysis of morphine and amphetamine in meconium with immunoassay and HPLC-diode-array detection. J. Anal. Toxicol. 18: 294-95 (1994).
8. C.X. Gao, T.Y. Chou, and I.S. Krull. Polymeric activated ester reagents for off-line and on-line derivatizations of amine nucleophiles in high-performance liquid chromatography with ultraviolet and fluorescence detection. Anal. Chem. 61: 1538-48 (1989).
9. P. Jakob, E.C. Tisdale, K. Panganiban, D. Cannon, K. Zabel, J.E. Mendelson, and R.T. Jones. Gas chromatographic determination of methamphetamine and its metabolite amphetamine in human plasma and urine following conversion to N-propyl derivatives. J. Chromatogr. 664: 449-57 (1995).
10. S. Dugan, S. Bogema, R.W. Schwartz, and N.T. Lappas. Stability of drugs of abuse in urine samples stored at -20°C, J. Anal. Toxicol. 18: 391-96 (1994).
11. R.J. Czarny and C.L. Hornbeck. Quantitation of methamphetamine and amphetamine in urine by capillary GC/MS. part II. derivatization with 4-carbethoxyhexafluorobutyryl chloride. J. Anal. Toxicol. 13: 257-62 (1989).
12. J.S. Fritz, P.J. Dumont, and L.W. Schmidt. Methods and materials for solid-phase extraction. J. Chromatogr. 691: 133-40 (1995).
13. P.G.M. Zweipfenning, A.H.C.M. Wilderink, P. Horsthuis, J.-P. Franke, and R.A. de Zeeuw. Toxicological analysis of whole blood samples by means of Bond-Elut Certify columns and gas chromatography with nitrogen-phosphorus detection. J. Chromatogr. 674: 87-95 (1994).
14. R. Melgar and R.C. Kelly. A novel GC/MS derivatization method for amphetamines. J. Anal. Toxicol. 17: 399-402 (1993).
15. H. Brzezinka, P. Dallakian, H. Budzikiewicz, M. Geissler, and A. Paul. GC-MS 15, Shimadzu Application Note (1995).
16. N. Kucharczyk. Estimation of the lower limit of quantitation, a method detection performance parameter for biomedical assays, from calibration curves. J. Chromatogr. 612: 71-76 (1993).
17. DIN 32645, Beuth Verlag, Berlin, 1991.
18. Clarke's Isolation and Identification of Drugs in Pharmaceuticals, Body Fluids, and Postmortem Materials 2nd ed. A.C. Moffat, Ed. The Pharmaceutical Press, London (1986).