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Based on the measurement of the sign and magnitude of optical specific rotation. The ee was also determined by transformation of 3 into the corresponding (R)-(+)-Mosher ester and checked by GC and NMR. See the previous report by Lin Guo-Qiang and Xu Wei Chu, Chinese J. of Chem. 1995, 13, 380.
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The reagent 10 was prepared according to the reference 7
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(a) The reagent 10 was prepared according to the reference 7.
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