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Volumn 37, Issue 11, 1996, Pages 1743-1746

A convenient procedure for the reduction of S-(+)-silyl serine methyl ester to chiral serinol derivatives

Author keywords

[No Author keywords available]

Indexed keywords

SERINE DERIVATIVE;

EID: 0029921898     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(96)00164-5     Document Type: Article
Times cited : (23)

References (28)
  • 4
    • 0003905731 scopus 로고    scopus 로고
    • ed. J. D. Morrison, Academic, New York
    • (d) Evans, D. A., Asymmetric Synthesis, ed. J. D. Morrison, Academic, New York, Vol. 3.
    • Asymmetric Synthesis , vol.3
    • Evans, D.A.1
  • 7
    • 33544461247 scopus 로고
    • U.S. Patent 3 935 280, Jan 27, 1976, 135101p.
    • (b) Lane, C. F., U.S. Patent 3 935 280, Jan 27, 1976, Chem Abstr. 1976, 84, 135101p.
    • (1976) Chem Abstr. , vol.84
    • Lane, C.F.1
  • 13
  • 16
    • 0027260325 scopus 로고
    • For examples see ref 1a., also Gonda, J.; Helland, A. C.; Ernst, B.; Bellus, D. Synthesis, 1993, 729. Sibi, M. P.; Rutherford, D.; Sharma, R. J. Chem. Soc. Perk. Trans. 1, 1994, 1675.
    • (1993) Synthesis , pp. 729
    • Gonda, J.1    Helland, A.C.2    Ernst, B.3    Bellus, D.4
  • 19
    • 85030188007 scopus 로고    scopus 로고
    • -1, 254 nm
    • -1, 254 nm
  • 21
    • 85030192766 scopus 로고    scopus 로고
    • note
    • 3) -6.2, -5.8, 17.93, 25.48, 51.64, 55.26, 65.16, 174.24.
  • 22
    • 85030195141 scopus 로고    scopus 로고
    • note
    • 5 of the hydroxymethyl oxazoline 5, to be 93-95%.
  • 25
    • 85030189261 scopus 로고    scopus 로고
    • HPLC analysis immediately following reduction gave a ratio of 96:4. After 2 weeks under the described storage conditions, a ratio of 94:6 was observed following formation of the oxazoline
    • HPLC analysis immediately following reduction gave a ratio of 96:4. After 2 weeks under the described storage conditions, a ratio of 94:6 was observed following formation of the oxazoline.
  • 27
    • 0000401335 scopus 로고
    • For conjugate addition to nonchelating 1-naphthyl oxazolines see Rawson, D. J.; Meyers, A. I. J. Org. Chem. 1991, 56, 2607. For additions to α,β-unsaturated acyclic nonchelating oxazolines see Shipman, M.; Meyers, A. I. J. Org. Chem. 1991, 56, 7098.
    • (1991) J. Org. Chem. , vol.56 , pp. 2607
    • Rawson, D.J.1    Meyers, A.I.2
  • 28
    • 0000200874 scopus 로고
    • For conjugate addition to nonchelating 1-naphthyl oxazolines see Rawson, D. J.; Meyers, A. I. J. Org. Chem. 1991, 56, 2607. For additions to α,β-unsaturated acyclic nonchelating oxazolines see Shipman, M.; Meyers, A. I. J. Org. Chem. 1991, 56, 7098.
    • (1991) J. Org. Chem. , vol.56 , pp. 7098
    • Shipman, M.1    Meyers, A.I.2


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.