(1R,5S)-(+)-nopinone of high enantiomeric purity

Synthetic Communications

Volumn 26, Issue 10, 1996, Pages 2027-2030

  Kozmina, Natasha ^a   Paquette, Leo A ^a  

^a OHIO STATE UNIVERSITY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

BETA PINENE; NOPINONE; UNCLASSIFIED DRUG;

ARTICLE; DRUG PURIFICATION; DRUG PURITY; ENANTIOMER; TECHNIQUE;

EID: 0029898717     PISSN: 00397911     EISSN: None     Source Type: Journal    
DOI: 10.1080/00397919608003558     Document Type: Article

References (6)

1. Boger, D. L., Mullican, M. D., Hellberg, M. R. and Patel, M. J. Org. Chem., 1985, 50, 1904.
2. Comyns, A. E. and Lucas, H. J., J. Am. Chem. Soc. 1957, 79, 4339.
3. 4 appears to be highly shock sensitive and exhibits extreme exothermic behavior with initiation temperatures below 65 °C. Consequently, a cautionary note is sounded regarding the safety precautions that must be exercised when working with the potentially hazardous complex.
4. Newman, M. S. "An Advanced Organic Laboratory Course," The Macmillan Company, 1972, Chapter 10.
5. 6
6. Brown, H. C., Weissman, S. A., Perumal, P. T. and Dhokte, U. P., J. Org. Chem. 1990, 55, 1217.