Synthesis of tributyltinmethylated sugars, building blocks for tethered reactions

Tetrahedron Letters

Volumn 37, Issue 24, 1996, Pages 4211-4212

  Hansen, Henrik C ^a   Hindsgaul, Ole ^a   Bols, Mikael ^b  

^a UNIVERSITY OF ALBERTA   (Canada)

^b AARHUS UNIVERSITY   (Denmark)

Author keywords

[No Author keywords available]

Indexed keywords

ALCOHOL; GLYCOSIDE; MANNOSIDE; METHYL IODIDE; TRIBUTYLTIN;

ACETYLATION; ARTICLE; PEPTIDE SYNTHESIS; PROTEIN CONFORMATION; PROTON NUCLEAR MAGNETIC RESONANCE; STEREOCHEMISTRY;

EID: 0029890722     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(96)00798-8     Document Type: Article

References (13)

1. a) Bols, M.; Skrydstrup, T. Chem. Rev. 1995 95 1253.
2. b) Valverde, S.; Gomez, A.M.; Hernandez, A. Herradon, B.; Lopez, J. C. J. Chem. Soc. Chem. Comm. 1995 2005 and references therein.
3. Still, W. C.; Mitra, A. J. Am. Chem. Soc. 1978 100 1927.
4. Hutchinson, D. K.; Fuchs, P. L. J. Am. Chem. Soc. 1987 109 4930.
5. Bols, M. Tetrahedron 1993 49 10049.
6. Seitz, D. E.; Carroll, J. J.; Cartaya, M.; Lee, S. -H.; Zapata, A. Synthetic Commun. 1983 13 129.
7. 3).
8. Paulsen, H. Carbohydr. Res. 1980 200 127.
9. Sawyer, J. S.; Narayanan, B. A. Synthetic Commun. 1983 13 135.
10. 2, drying, concentration and flash-chromatography gave 3.21 g 4 (66%).
11. Holick, S. A.; Anderson, L. Carbohydr. Res. 1974 34 208.
12. The mass spectrum gave m/z: 567 (M + Na), 544 (M+).
13. 2's).