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note
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Without prior protection of the allylic hydroxyl group, compounds 13 and 14 were the only two products isolated when the THP ether 6 was subjected to the acidic conditions mentioned in the text. formula presented
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27
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85030205496
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note
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AB = 12.5 Hz, both d with J = 8 and 4 Hz, respectively), 4.36 (t, 1H, J = 6.5 Hz), 5.50 (dd, 1H, J = 7.5, 15.5 Hz), 5.94 (dt, 1H, J = 15.5 Hz (d), 7 Hz (t)).
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