Generation of rhodium carbenoids on a polystyrene support and their OH-insertion reaction with alcohols

Tetrahedron

Volumn 52, Issue 16, 1996, Pages 5999-6002

  Zaragoza, Florencio ^a   Petersen, Susanne Vejle ^a  

^a NOVO NORDISK A S   (Denmark)

Author keywords

[No Author keywords available]

Indexed keywords

ETHER DERIVATIVE; PIPERAZINE DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; PRIORITY JOURNAL; REACTION ANALYSIS;

EID: 0029882001     PISSN: 00404020     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4020(96)00230-X     Document Type: Article

References (16)

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2. Ye, T.; McKervey, M. A. Chem. Rev. 1994, 94, 1091-1160; Adams, J.; Spero, D. M. Tetrahedron 1991, 47, 1765-1808.
3. See e. g. Stork, G.; Nakatani, K. Tetrahedron Lett. 1988, 29, 2283-2286.
4. a) Zaragoza, F. Tetrahedron Lett. 1995, 36, 8677-8678;
5. b) Dixit, D. M.; Leznoff, C. C. J. Chem. Soc., Chem. Commun. 1977, 798-799.
6. Rothe, M.; Zieger, M. Tetrahedron Lett. 1994, 35, 9011-9012; Hiroshige, M; Hauske, J. R.; Zhou, P. J. Am. Chem. Soc. 1995, 117, 11590-11591.
7. Rothe, M.; Zieger, M. Tetrahedron Lett. 1994, 35, 9011-9012; Hiroshige, M; Hauske, J. R.; Zhou, P. J. Am. Chem. Soc. 1995, 117, 11590-11591.
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9. Böhshar, M.; Fink, J.; Heydt, H.; Wagner, O.; Regitz, M. in Houben-Weyl, Vol. EI4b (Eds.: Klamann, D.; Hagemann, H.), Thieme, Stuttgart, New York, 1990, pp. 1069-1083, 1255-1256.
10. 1H NMR, IR), but no satisfactory elemental analyses could be obtained neither from the diazoamide nor from derivatives thereof.
11. Miller, D. J.; Moody, C. J. Tetrahedron 1995, 51, 10811-10843; Cox, G. G.; Miller, D. J.; Moody, C. J.; Sie, E.-R. H. B.; Kulagowski, J. J. Tetrahedron 1994, 50, 3195-3212; Hlaváček, J.; Král, V. Collect. Czech. Chem. Commun. 1992, 57, 525-530.
12. Miller, D. J.; Moody, C. J. Tetrahedron 1995, 51, 10811-10843; Cox, G. G.; Miller, D. J.; Moody, C. J.; Sie, E.-R. H. B.; Kulagowski, J. J. Tetrahedron 1994, 50, 3195-3212; Hlaváček, J.; Král, V. Collect. Czech. Chem. Commun. 1992, 57, 525-530.
13. Miller, D. J.; Moody, C. J. Tetrahedron 1995, 51, 10811-10843; Cox, G. G.; Miller, D. J.; Moody, C. J.; Sie, E.-R. H. B.; Kulagowski, J. J. Tetrahedron 1994, 50, 3195-3212; Hlaváček, J.; Král, V. Collect. Czech. Chem. Commun. 1992, 57, 525-530.
14. Treatment of the 2-diazo-3-oxobutyramide 2 with rhodium(II) acetate in the presence of benzylalcohol yielded, after cleavage from the support, a complex mixture of products.
15. Nicoud, J.-F.; Kagan, H. B. Tetrahedron Lett. 1971, 2065-2068.
16. Shimamoto, K.; Ishida, M.; Shinozaki, H.; Ohfune, Y. J. Org. Chem. 1991, 56, 4167-4176.