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13344250070
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note
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Integration of the crude reaction mixture was performed using fluorobenzene as an internal standard. The perfluoronaphthalene was isolated following chromatography on silica with pentane. The fraction was collected, and rotatory evaporation yielded 0.665 g (2.44 mmol. 4%) of White crystalline perfluoronaphthalene.
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24
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13344284259
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note
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19F NMR spectroscopy using added fluorobenzene as an internal standard.
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25
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33845183302
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(a) Negishi, E.; Holmes, S. J.; Tour, J. M.; Miller, J. A.; Cederbaum, F. E.; Swanson, D. R.; Takahashi, T. J. Am. Chem. Soc. 1989, 111, 3336-3346.
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Miller, J.A.4
Cederbaum, F.E.5
Swanson, D.R.6
Takahashi, T.7
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26
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13344283027
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note
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19F NMR spectroscopy. A control experiment showed that there is no reaction between n-BuLi and perfluorodecalin.
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28
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0002470392
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(b) Rausch, M D ; Boon, W. H.; Mintz, E. A. J. Organomet. Chem. 1978, 160, 81-92.
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31
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13344249359
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note
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19F NMR spectroscopy using added fluorobenzene as an internal standard.
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33
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37049087412
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Burk, M. J., Staley, D. L., Tumas, W. J. Chem Soc., Chem. Commun. 1990, 809-810.
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