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85030192664
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The methyl ester formed initially cyclized (trans-esterified) to form the lactone immediately.
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85030189787
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32 derivative of the reduced diol failed.
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32
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85030189679
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note
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19F NMR spectum of the bis-MTPA ester of the racemic diol shows 4 peaks at δ 72.61, 72.75, 72.90 and 73.02. The di-ester of the reduction product shows only two peaks at δ 72.61 and 72.90, corresponding to the R-isomer as determined by comparing the rotation with that reported in the literature. To be within the margin of error allowed in analyses using NMR spectroscopy, we report ≥96% ee.
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34
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0343670168
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