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Volumn 37, Issue 17, 1996, Pages 3001-3004

Application of D,L-FDLA derivatization to determination of absolute configuration of constituent amino acids in peptide by advanced Marfey's method

Author keywords

[No Author keywords available]

Indexed keywords

AERUGINOPEPTIN 228 A; CYANOGINOSIN LR; UNCLASSIFIED DRUG;

EID: 0029876115     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(96)00484-4     Document Type: Article
Times cited : (104)

References (14)
  • 10
    • 85030190696 scopus 로고    scopus 로고
    • note
    • The usual acid hydrolysis of 2 with 6 N HCl at 110°C for 12 hrs gave completely racemized pentahomoserine and Pro.
  • 11
    • 85030197255 scopus 로고    scopus 로고
    • note
    • The derivatized hydrolysate of 2 with D-and L-FDLA was analyzed by ESI LC/MS under the following conditions: LC, column, Develosil ODS-HG-5 (150 x 2.0 mm I.D., Nomura Chemical, Seto Japan); mobile phase, A) H2O containing 0.01 M TFA, B) CH3CN; gradient rate, A) : B) = 7:3 -> 3:7 (40 min), linear; flow rate, 0.2 ml/min : MS, TSQ7000 (Finnigan MAT, California, U.S.A.).


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.