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85030190696
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note
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The usual acid hydrolysis of 2 with 6 N HCl at 110°C for 12 hrs gave completely racemized pentahomoserine and Pro.
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11
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85030197255
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note
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The derivatized hydrolysate of 2 with D-and L-FDLA was analyzed by ESI LC/MS under the following conditions: LC, column, Develosil ODS-HG-5 (150 x 2.0 mm I.D., Nomura Chemical, Seto Japan); mobile phase, A) H2O containing 0.01 M TFA, B) CH3CN; gradient rate, A) : B) = 7:3 -> 3:7 (40 min), linear; flow rate, 0.2 ml/min : MS, TSQ7000 (Finnigan MAT, California, U.S.A.).
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0020445340
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37049101108
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Botes, D. P.; Wessels, P. L.; Kruger, H.; Runneger M. T. C.; Santikarn, S.; Smith, R. J.; Barna, J. C. J.; Williams, D. H. J. Chem. Soc. Perkin Trans. I, 1985, 2747-2748.
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