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85030192707
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note
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8 (0.25 mmol) in freshly distilled benzene (10 mL) was stirred under 1000 psi of carbon monoxide at 120 °C for 24 h. The solvent was removed by rotary evaporation, and the product (2) was purified by chromatography on silica gel with 5:1 hexane:ether as the eluant
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30
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85030192691
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note
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14 Similarly, 1e was prepared in 83 % yield.
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0002990104
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