Bi- and tricyclic penta- and hexacoordinated phosphoranes with varying ring sizes: Synthesis, structures, and reactivity

Journal of the American Chemical Society

Volumn 118, Issue 41, 1996, Pages 9841-9849

  Said, Musa A ^a   Pülm, Melanie ^b   Herbst Irmer, R ^b   Swamy, K C Kumara ^a  

^a UNIVERSITY OF HYDERABAD   (India)

^b UNIVERSITY OF GÖTTINGEN   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

ORGANOPHOSPHORUS COMPOUND;

ARTICLE; CRYSTALLOGRAPHY; DRUG STRUCTURE; DRUG SYNTHESIS; NUCLEAR MAGNETIC RESONANCE; REACTION ANALYSIS;

EID: 0029859435     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja960554v     Document Type: Article

References (41)

1. (a) Huang, Y.; Arif, A. M.; Bentrude, W. G. J. Am. Chem. Soc. 1991, 113, 7800.
2. (b) Huang, Y.; Sopchik, A. E.; Arif, A. M.; Bentrude, W. G., J. Am. Chem. Soc. 1993, 115, 6235.
3. (c) Schomburg, D.; Hacklin. H.; Roschenthaler, G. V. Phosphorus Sulfur 1988, 35, 241.
4. (d) Prakasha, T. K.; Day, R. O.; Holmes, R. R. J. Am. Chem. Soc. 1994, 116, 8095.
5. (e) Hans, J.; Day, R. O.; Howe. L.; Holmes, R. R. Inorg. Chem. 1992, 31, 1279.
6. (f) Burton, S. D.; Kumara Swamy, K. C.; Holmes, J. M.; Day, R. O.; Holmes, R. R. J. Am. Chem. Soc. 1990, 112, 6104.
7. (g) Day, R. O.; Kumara Swamy, K. C.; Fairchild, L.; Holmes. J. M.; Holmes. R. R. J. Am. Chem. Soc. 1991, 113, 1627.
8. (h) Holmes, R. R.; Kumara Swamy, K. C.; Holmes, J. M.; Day, R. O. Inorg. Chem. 1991, 30, 1052.
9. (i) Timosheva, N. V.; Prakasha, T. K.; Chandrasekaran, A.; Day, R. O.: Holmes, R. R. Inorg. Chem. 1995, 34, 4525.
10. (a) Prakasha, T. K.; Day, R. O.; Holmes, R. R. Inorg. Chem. 1992, 31, 725, 1913, 3391.
11. (b) Prakasha. T. K.; Day, R. O.; Holmes, R. R. J. Am. Chem. Soc. 1993, 115, 2690.
12. (a) Fluck, E.; Heckmann, G. In Phosphorus-31 NMR Spectroscopy in Stereochemical Analysis; Verkade, J. G., Quin, L. D.. Eds.; VCH: Deerfield Beach, Florida, 1987; Chapter 2.
13. (b) Criegern, T. V.; Schmidpeter, A. Phosphorus Sulfur 1979, 7, 305.
14. (c) Cong, C. B.; Gence, G.; Garrigues, B.; Koenig, M.; Munoz, A. Tetrahedron 1979, 35, 1825.
15. (d) Koenig, M.; Khatib, F. E.; Munoz, A.; Wolf, R. Tetrahedron Lett. 1982, 23, 421.
16. (e) Shevchenko, I. V. Tetrahedron Lett. 1995, 36, 2021.
17. (f) John, K. P.; Schmutzler, R.; Sheldrick, W. S. J. Chem. Soc., Dalton Trans. 1974, 1841.
18. (g) John. K. P.; Schmutzler, R.; Sheldrick, W. S. J. Chem. Soc., Dalton Trans. 1974, 2466.
19. Shevchenko, I. V.; Fischer, A.; Jones, P. G.; Schmutzler, R. Chem. Ber. 1992, 125, 1325.
20. Said, M. A.; Kumara Swamy, K. C.; Chandra Mohan, K.; Venkata Lakshmi, N. Tetrahedron 1994, 50, 6989.
21. Said, M. A.; Kumara Swamy, K. C.; Veith, M.; Huch, V. J. Chem. Soc., Perkin Trans, 1 1995, 2945.
22. Said. M. A.; Kumara Swamy, K. C.; Veith, M.; Huch, V., submitted for publication.
23. Holmes, R. R.; Deiters, J. A. Inorg. Chem. 1994, 33, 3235.
24. Perrin, D. D.; Armarego, W. L. F.; Perrin, D. R. Purification of Laboratory Chemicals; Pergamon, Oxford, 1986.
25. Gallucci, J. C.; Holmes, R. R. Inorg. Chem. 1980, 19, 3540.
26. Sheldrick, G. M. SHELXS-90. Acta Crystallogr. 1990, A46, 467.
27. Sheldrick, G. M. SHELXL-93, University of Göttingen, 1993.
28. (a) Flack, H. D. Acta Crytallogr. 1983, A39, 876.
29. (b) Pratt, C. S.; Coyle, B. A.; Ibers, J. A. J. Chem. Soc. 1971, 2146.
30. Sarma, R.; Ramirez, F.; Mckeever, B.; Marecek, J. F.; Lee, S. J. Am. Chem. Soc. 1976, 98, 581.
31. Kumara Swamy, K. C.; Day, R. O.; Holmes, J. M.; Holmes, R. R. J. Am. Chem. Soc. 1990, 112, 6095.
32. Said, M. A.; Kumara Swamy, K. C., Unpublished data.
33. Prakasha, T. K.; Burton, S. D.; Day, R. O.; Holmes, R. R. Inorg. Chem. 1992, 31, 5494.
34. Prakasha, T. K.; Chandrasekaran, A.; Day, R. O.; Holmes, R. R. Inorg. Chem. 1995, 34, 1243 and the references cited therein.
35. Koenig, M.; Klaebe, A.; Munoz, A.; Wolf, R. J. Chem. Soc., Perkin Trans. 2 1979, 40.
36. Hellwinkel, D.; Lindner, W.; Wilfinger, H. J. Chem. Ber. 1974, 107, 1428.
37. Holmes, R. R.; Prakasha, T. K.; Pastor, S. D. in Phosphorus-31 NMR Spectral Properties in Compound Characterization and Structural Analysis; Quin. L. D., Verkade, J. G., Eds; VCH: New York, 1994; Chapter 3.
38. Blom, R.; Haaland, A. J. Mol. Strukt. 1985, 128, 21.
39. Boessenkool, I. K.; Boeyens, J. C. A. J. Cryst. Mol. Struct. 1980, 10, 11.
40. Gould, R. O.; Taylor, P. PUCKER Program for the calculation of ring conformations, University of Edinburgh, 1994.
41. Emsley, J. Die Elemente: W. de Gruyter: Berlin, 1994.