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Volumn 118, Issue 36, 1996, Pages 8751-8752

Chiral recognition is observed in the deprotonation reaction of cytochrome c by (2R)- and (2S)-2-butylamine

Author keywords

[No Author keywords available]

Indexed keywords

BUTYLAMINE; CYTOCHROME C;

EID: 0029847279     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja960686o     Document Type: Article
Times cited : (39)

References (49)
  • 9
    • 10144225550 scopus 로고    scopus 로고
    • note
    • -5 M solution of cytochrome c dissolved in 50:50 water/methanol.
  • 10
    • 10144224849 scopus 로고    scopus 로고
    • note
    • Unless noted, the desired charge state was selected by ejection of other ions produced from the electrospray source using standard FTMS procedures.
  • 37
    • 10144247180 scopus 로고    scopus 로고
    • note
    • The rate constants were obtained by examining the decay of the sum of the charge state and the adduct intensities relative to the resulting charge reduced state and its corresponding adduct. The adducted species is found to be the intermediate in the reaction. Isolating this ion produced the deprotonated (adducted and unadducted) species after a period of time.
  • 38
    • 10144239598 scopus 로고    scopus 로고
    • note
    • Experimental details of the ion gauge calibration are provided in earlier publications. See refs 7 and 8.
  • 39
    • 10144243246 scopus 로고
    • Unpublished results
    • Wu, J.; Lebrilla, C. B. 1995, Unpublished results.
    • (1995)
    • Wu, J.1    Lebrilla, C.B.2
  • 44
    • 0000849231 scopus 로고
    • Cassady, C. J.; Wronka, J.; Kruppa, G. H.; Laukien, F. H. Rapid Commun. Mass Spectrom. 1994, 8, 394-400. See also: Schnier, P. D.; Gross, D. S.; Williams, E. R. J. Am. Chem. Soc. 1995, 117, 6747-6757.
    • (1995) J. Am. Chem. Soc. , vol.117 , pp. 6747-6757
    • Schnier, P.D.1    Gross, D.S.2    Williams, E.R.3
  • 46
    • 10144233385 scopus 로고    scopus 로고
    • note
    • As a caveat, we find that the rates are extremely sensitive to source conditions, as others have pointed out (see, for example, ref 40). When we modified the ESI source affecting the skimmer diameter and pumping between the stages, we found that the fast-reacting components dissappeared.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.