Highly symmetric group 13 metal-phospinato complexes: Multinuclear NMR (27Al, 31P, 71Ga) determination of stability constants at low pH

Journal of the American Chemical Society

Volumn 118, Issue 43, 1996, Pages 10446-10456

  Lowe, Mark P ^a   Rettig, Steven J ^a   Orvig, Chris ^a  

^a UNIVERSITY OF BRITISH COLUMBIA   (Canada)

Author keywords

[No Author keywords available]

Indexed keywords

ALUMINUM; GALLIUM; INDIUM; METAL COMPLEX;

ARTICLE; COMPLEX FORMATION; DRUG STABILITY; DRUG STRUCTURE; NUCLEAR MAGNETIC RESONANCE; PH; X RAY CRYSTALLOGRAPHY;

EID: 0029818339     PISSN: 00027863     EISSN: None     Source Type: Journal    
DOI: 10.1021/ja961633+     Document Type: Article

References (56)

1. (a) Wong, E.; Caravan, P.; Liu, S.; Rettig, S.; Orvig, C. Inorg. Chem. 1996, 35, 715.
2. (b) Wong, E.; Liu, S.; Lügger, T.; Hahn, F. E.; Orvig, C. Inorg. Chem. 1995, 34, 93.
3. (c) Liu, S.; Wong, E.; Karunaratne, V.; Rettig, S. J.; Orvig, C. Inorg. Chem. 1993, 32, 1756.
4. (d) Liu, S.; Wong, E.; Rettig, S. J.; Orvig, C. Inorg. Chem. 1993, 32, 4268.
5. (e) Liu, S.; Rettig, S. J.; Orvig, C. Inorg. Chem. 1992, 31, 5400.
6. (a) Perl, D. P. Environ. Health Perspect. 1985, 63, 149.
7. (b) Crapper-McLachlan, D. R. Neurobiol. Aging 1986, 7, 525.
8. (c) Liss, L. Aluminum Neurotoxicity; Pathotox Publishers: Park Forest, IL, 1980.
9. (a) Welch, M. J.; Moerlein, S. M. In Inorganic Chemistry in Biology and Medicine; Martell, A. E, Ed.; American Chemical Society: Washington, DC, 1980; p 121.
10. (b) Green, M. A.; Welch, M, J. Nucl. Med. Biol. 1989, 16, 435.
11. (c) Zhang, Z.; Lyster, D. M.; Webb, G. A.; Orvig, C. Nucl. Med, Biol. 1992, 19, 327.
12. Yang, L.-W.; Liu, S.; Wong, E.; Rettig, S. J.; Orvig, C. Inorg. Chem. 1995, 34, 2164.
13. (a) Kiss, T.; Lázár, I.; Kafarski, P. Met.-Based Drugs 1994, 1, 247.
14. (b) Jezowska-Bojczuk, M.; Kiss, T.; Kozlowski, H.; Decock, P.; Barycki, J. J. Chem. Soc., Dalton Trans. 1994, 811.
15. (a) Hermann, P.; Lukeš, I. J. Chem. Soc., Dalton Trans. 1995, 2605.
16. (b) Hermann, P.; Lukeš, I.; Vojtíšek, P.; Císarová, I. J. Chem. Soc., Dalton Trans. 1995, 2611.
17. (a) Lázár, I.; Sherry, A. D.; Ramasamy, R.; Brücher, E.; Kiraly, R. Inorg. Chem. 1991, 30, 5016.
18. (b) Lázár, I.; Ramasamy, R.; Brücher, E.; Geraldes, C. F. G. C.; Sherry, A. D. Inorg. Chim. Acta 1992, 195, 89.
19. (a) Aime, S.; Batsanov, A. S.; Botta, M.; Howard, J. A. K.; Parker, D.; Senanayake, K.; Williams, G. Inorg. Chem. 1994, 33, 4696.
20. (b) Aime, S.; Botta, M.; Parker, D.; Williams, J. A. G. J. Chem. Soc., Dalton Trans. 1995, 2259.
21. Bollinger, J. E.; Roundhill, D. M. Inorg. Chem. 1993, 32, 2821.
22. Cole, E.; Copley, R. C. B.; Howard, J. A. K.; Parker, D.; Ferguson, G.; Gallagher, J. F.; Kaitner, B.; Harrison, A.; Royle, L. J. Chem. Soc., Dalton Trans. 1994, 1619.
23. (a) Dellavia, I.; Blixt, J.; Dupressoir, C.; Detellier, C. Inorg. Chem. 1994, 33, 2823.
24. (b) Karlik, S. J.; Elgavish, G. A.; Eichhorn, G. L. J. Am. Chem. Soc. 1983, 105, 602.
25. (c) Feng, Q.; Waki, H.; Kura, G. Polyhedron 1991, 10, 1527.
26. (d) Karlik, S. J.; Elgavish, G. A.; Pillai, R. P.; Eichhorn, G. L. J. Magn. Reson. 1982, 49, 164.
27. (e) Bock, J. L.; Ash, D. E. J. Inorg. Biochem. 1980, 13, 105.
28. (a) Hinton, J. F.; Briggs, R. W. NMA and the Periodic Table; Harris, R. K., Mann, B. E., Eds.; Academic: London, 1978; pp 279-303.
29. (b) Akitt, J. W. Prog. Nucl. Magn. Reson. Spectros. 1989, 21, 1.
30. Schmidt, H.; Lensink, C.; Xi, S. K.; Verkade, J. G. Z Anorg. Allg. Chem. 1989, 578, 75.
31. Moedritzer, K.; Irani, R. R. J. Org. Chem. 1966, 31, 1603.
32. Caravan, P.; Hedlund, T.; Liu, S.; Sjöberg, S.; Orvig, C. J. Am. Chem. Soc: 1995, 117, 11230.
33. teXsan; Crystal Structure Analysis Package (1985 & 1992); Molecular Structure Corporation: The Woodlands, TX.
34. International Tables for X-Ray Crystallography, Kynoch Press: Birmingham, England, 1974; Vol. IV, pp 99-102.
35. International Tables for Crystallography; Kluwer Academic Publishers: Boston, MA. 1992; Vol. C. pp 200-206.
36. Geraldes, C. F. G. C.; Brücher, E.; Cortes, S.; Koenig, S. H.; Sherry, A. D. J. Chem. Soc., Dalton Trans. 1992, 2517.
37. Martell, A. E.; Smith, R. M. Critical Stability Constants; Plenum: New York, 1974-1989; Vols. 1-6.
38. Geraldes, C. F. G. C.; Sherry, A. D.; Cacheris, W. P. Inorg. Chem. 1989, 28, 3336.
39. Liu, S.; Yang. L.-W.; Rettig, S. J.; Orvig, C. Inorg. Chem. 1993, 32, 2773.
40. Lowe, M. P.; Lockhart, J. C.; Matthews, C. J.; Clegg, W.; Elsegood, M. R. J.; Horsburgh, L. J. Chem. Soc., Perkin Trans. 2 1994, 1957.
41. Günther, H. NMR Spectroscopy; John Wiley and Sons: New York, 1985; pp 180-181.
42. Abraham, R. J.; Gatti, G. J. J. Chem. Soc., B 1969, 961.
43. Delpuech J.-J. NMR of Newly Accessible Nuclei; Laszlo, P., Ed.; Academic Press: New York, 1983: Vol. 2. pp 153-195.
44. Finnegan, M.; Lutz, T. G.; Nelson, W. O.; Smith, A.; Orvig, C. Inorg. Chem. 1987, 26, 2171.
45. Greenwood, N. N.; Earnshaw, A. Chemistry of the Elements; Pergamon: Toronto, 1987; p 1434.
46. Caravan, P.; Orvig. C. Submitted for publication.
47. Shannon, R. D. Acta Crystallogr. 1976, A32, 751.
48. Hegetschweiler, K.; Kradolfer, T.; Gramlich, V.; Hancock, R. D. Chem. Eur. J. 1995, 1, 74.
49. Orvig, C. Coordination Chemistry of Aluminum; Robinson, G., Ed.; VCH Publishers Inc.: New York, 1993; pp 85-121.
50. (a) Delpuech, J.-J.; Khaddar, M. R.; Peguy, A. A.; Rubini, P. R. J. Am. Chem. Soc. 1975, 97, 3373.
51. (b) Delpuech, J.-J.; Khaddar, M. R.; Peguy, A. A.; Rubini, P. R. J. Chem. Soc., Chem. Commun. 1974, 154.
52. Rubini, P. R.; Rodehüser, L.; Delpuech, J.-J. Inorg. Chem. 1979, 18, 2962.
53. (a) Van Vriezen, N. H. W.; Jellinek, F. Chem. Phys. Lett. 1967, 1, 284.
54. (b) Van Vriezen, N. H. W.; Jellinek, F. Recl. Trav. Chim. Pays-Bas 1970, 89, 1306.
55. (c) Laussac, J.-P.; Laurent, J. P. J. Chim. Phys. 1973, 70, 417.
56. (d) Laussac, J.-P.; Laurent, J. P.; Commenges, G. Org. Magn. Reson. 1975, 7, 72.