Determination of plasma total homocysteine and cysteine using HPLC with fluorescence detection and an ammonium 7-fluoro-2, 1, 3-benzoxadiazole-4-sulphonate (SBD-F) derivatization protocol optimized for antioxidant concentration, derivatization reagent concentration, temperature and matrix pH

Biomedical Chromatography

Volumn 10, Issue 5, 1996, Pages 205-212

  Daskalakis, I ^a   Lucock, M D ^a   Anderson, A ^b   Wild, J ^a   Schorah, C J ^a   Levene, M I ^a  

^a LEEDS GENERAL INFIRMARY   (United Kingdom)

^b GLASGOW ROYAL INFIRMARY   (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

BLOOD; CALIBRATION; DIGITAL STORAGE; FLUORESCENCE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; METABOLISM; SILICA;

ANTIOXIDANT CONCENTRATION; DERIVATIZATION REAGENT; DERIVATIZATIONS; FLUORESCENCE DETECTION; HOMOCYSTEINES; INTERNAL STANDARDS; MATRIX; MOBILE PHASIS; REAGENT CONCENTRATION; SULPHONATES;

AMINO ACIDS;

ACETONITRILE; AMMONIUM 7 FLUORO 2,1,3 BENZOXADIAZOLE 4 SULFONATE; ANTIOXIDANT; CYSTEINE; CYSTEINE DERIVATIVE; CYSTEINYLGLYCINE; EDETIC ACID; HEPARIN; HOMOCYSTEINE; LITHIUM; REAGENT; REDUCING AGENT; SULFONIC ACID DERIVATIVE; THIOL; UNCLASSIFIED DRUG;

ARTICLE; BLOOD LEVEL; BLOOD PH; CALIBRATION; DERIVATIZATION; ERYTHROCYTE METABOLISM; FLUORESCENCE; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; PH; STANDARD; TEMPERATURE;

EID: 0029813018     PISSN: 02693879     EISSN: None     Source Type: Journal    
DOI: 10.1002/(SICI)1099-0801(199609)10:5<205::AID-BMC589>3.0.CO;2-P     Document Type: Article

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