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With protected purines (1b,d,e,f), about 80% of the starting material was consumed under the conditions described in the Experimental Section. For reaction with purines la,c in EtOH, larger amounts of starting material could be recovered from the reaction mixture. Longer reaction times, however, revealed the formation of side products in detriment of the yield of the C(8)-fluorinated products. Also, solvents such as water and HOAc provided much lower yields than that observed in EtOH medium.
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3): δ-108.2 ppm] consistent with unaltered 2c. Srinivasan, A.; Gambhir, S.; Barrio, J. R.; Wu, L.; Namavari, M.; Satyamurthy, N.; Sharfstein, S.; Cherry, S.; Green, A.; Berk, A.; Phelps, M. E.; Herschman, H.R. Submitted for publication in Science.
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Science
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Srinivasan, A.1
Gambhir, S.2
Barrio, J.R.3
Wu, L.4
Namavari, M.5
Satyamurthy, N.6
Sharfstein, S.7
Cherry, S.8
Green, A.9
Berk, A.10
Phelps, M.E.11
Herschman, H.R.12
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63
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0004104924
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Matheson: East Rutherford, NJ
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Matheson Gas Data Book; Braker, W., Mossman, A. L., Eds.; Matheson: East Rutherford, NJ, 1971; p 261.
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(1971)
Matheson Gas Data Book
, pp. 261
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Braker, W.1
Mossman, A.L.2
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64
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0018838514
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Barrio, J. R.; Bryant, J. D.; Keyser, G. E. J. Med. Chem. 1980, 23, 572.
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(1980)
J. Med. Chem.
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, pp. 572
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Barrio, J.R.1
Bryant, J.D.2
Keyser, G.E.3
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66
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0023917583
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Matsumoto, H.; Kaneko, C.; Yamada, K.; Takeuchi, T.; Mori, T.; Mizuno, Y. Chem. Pharm. Bull. 1988, 36, 1153.
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(1988)
Chem. Pharm. Bull.
, vol.36
, pp. 1153
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Matsumoto, H.1
Kaneko, C.2
Yamada, K.3
Takeuchi, T.4
Mori, T.5
Mizuno, Y.6
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67
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10544222299
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note
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2O, 60:36:4)). Optimum reaction times for product (2a,c) isolation varied from 2 to 5 h.
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