A practical photochemical synthesis of 6-aza-1,10-phenanthroic anhydride

Synthetic Communications

Volumn 26, Issue 19, 1996, Pages 3645-3652

  Pierce, Michael E ^a   Fortunak, Joseph M D ^a   Islam, Qamrul ^a  

^a DUPONT COMPANY   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

ANTINEOPLASTIC AGENT; DMP 315; PHENANTHRENE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; DRUG SYNTHESIS; PHOTOCHEMISTRY; REACTION ANALYSIS; TECHNIQUE;

EID: 0029789416     PISSN: 00397911     EISSN: None     Source Type: Journal    
DOI: 10.1080/00397919608003778     Document Type: Article

References (11)

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2. Patten, A. D.; Pacofsky, G. J.; Seitz, S. P.; Akamike, E. A.; Cherney, R. J.; Kaltenbach, R. F.; Orwat, M. J. U. S. Patent Application Serial Number 08/080862; Chem. Abstr. 1995, 123, 228003.
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6. Dimethyl homophthalate was used as a crude oil, prepared in quantitative yield by reacting homophthalic acid with thionyl chloride in methanol followed by removing solvent, diluting with t-butyl methyl ether, washing with aqueous sodium bicarbonate and removing solvent.
7. Timmons, C. J.; Loader, C. E. J. Chem. Soc.(C) 1966, 1078.
8. Sargent, M. V.; Timmons, C. J. J. Am. Chem. Soc. 1963, 85, 2186.
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10. Fehn, H.; Perkampus, H.-H. Tetrahedron 1978, 34, 1971.
11. The dihydrodiacid analog of 9 decarboxylated under photolysis.