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For specific examples of funetionalized TTF derivatives where π-π stacking has been established by X-ray crystal structures see: a) C. Nakano, K. Imaeda, T. Mori, Y. Muruyama, H. Inokuchi, N. Iwasawa, G. Saito, J. Mater. Chem. 1991, 1, 37. b) J. Garín, J. Orduna, S. Uriel, A. J. Moore, M. R. Bryce, S. Wegener, D. S. Yufit, J. A. K. Howard, Synthesis 1994, 489. c) A. S. Batsanov, N. Svenstrup, J. Lau, J. Becher, M. R. Bryce, J. A. K. Howard, J. Chem. Soc., Chem. Commun. 1995, 1201.
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0028302223
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For specific examples of funetionalized TTF derivatives where π-π stacking has been established by X-ray crystal structures see: a) C. Nakano, K. Imaeda, T. Mori, Y. Muruyama, H. Inokuchi, N. Iwasawa, G. Saito, J. Mater. Chem. 1991, 1, 37. b) J. Garín, J. Orduna, S. Uriel, A. J. Moore, M. R. Bryce, S. Wegener, D. S. Yufit, J. A. K. Howard, Synthesis 1994, 489. c) A. S. Batsanov, N. Svenstrup, J. Lau, J. Becher, M. R. Bryce, J. A. K. Howard, J. Chem. Soc., Chem. Commun. 1995, 1201.
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0141795148
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For specific examples of funetionalized TTF derivatives where π-π stacking has been established by X-ray crystal structures see: a) C. Nakano, K. Imaeda, T. Mori, Y. Muruyama, H. Inokuchi, N. Iwasawa, G. Saito, J. Mater. Chem. 1991, 1, 37. b) J. Garín, J. Orduna, S. Uriel, A. J. Moore, M. R. Bryce, S. Wegener, D. S. Yufit, J. A. K. Howard, Synthesis 1994, 489. c) A. S. Batsanov, N. Svenstrup, J. Lau, J. Becher, M. R. Bryce, J. A. K. Howard, J. Chem. Soc., Chem. Commun. 1995, 1201.
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24
-
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4243066158
-
-
note
-
max [DMF, 25 °C (ε)] 272 (56,500), 336 (27,900), 647 (13,400) and 677 (13,300); (DMF, 0 °C) 330 (shoulder) (15,500) 638 (8,589) and 670 (8.645); (DMF, 25 °C, after addition of an excess of iodine) 646 (11,754), 676 (11,800) and 880 (2,725) nm.
-
-
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25
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0001305809
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26
-
-
4243134774
-
-
note
-
Compound 6, a brown solid, m.p. 195 °C (from hexane) was prepared in 34 % yield by reaction of compound 1 with 4-nitrophthalonitrile in DMF in the presence of potassium carbonate (60-70 °C, 3 days).
-
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27
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0000786068
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