29Si MAS NMR spectrum and superstructure of modulated tridymite L3-To(MX-1)

European Journal of Mineralogy

Volumn 8, Issue 1, 1996, Pages 103-113

  Graetsch, Heribert ^a   Topalovic Dierdorf, Ivana ^a  

^a RUHR UNIVERSITY BOCHUM   (Germany)

Author keywords

29Si MAS NMR spectroscopy; Incommensurate modulation; SiO2; Tridymite

Indexed keywords

MODULATION; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; SILICATE MINERALS; SILICON OXIDES; SINGLE CRYSTALS;

INCOMMENSURATE MODULATION; LONGITUDINAL WAVES; MAS NMR; MAS-NMR SPECTROSCOPY; SILICON ATOMS; SINGLE CRYSTAL X-RAY DIFFRACTION; SIO2; TRIDYMITE;

SILICA;

INCOMMENSURATE MODULATION; MAS NMR; SPECTROSCOPY; TRIDYMITE;

EID: 0029756233     PISSN: 09351221     EISSN: None     Source Type: Journal    
DOI: 10.1127/ejm/8/1/0103     Document Type: Article

References (30)

1. Ashworth, J.R. (1989): Transmission electron microscopy of coexisting low-tridymite polymorphs. Mineral. Mag., 53, 89-97.
2. Baerlocher, Ch., Hepp, A., Meier, W.M. (1977): DLS-76 (Program for the simulation of crystal structures by geometric refinement).
3. Baur, W.H. (1977): Silicon-oxygen bond lengths, bridging angles Si-O-Si and synthetic low tridymite. Acta Cryst., B33, 2615-2619.
4. _ (1980): Straight Si-O-Si bridging bonds do exist in silicates and silicon dioxide polymorphs. Acta Cryst., B36, 2198-2202.
5. Cellai, D., Carpenter, M.A., Kirkpatrick, R.J., Salje, E.K.H., Zhang, M. (1995): Thermally induced phase transitions in tridymite: an infrared spectroscopy study. Phys. Chem. Minerals, 22, 50-60.
6. Dollase, W.A. (1967): The crystal structure at 220°C of orthorhombic high tridymite from the Steinbach meteorite. Acta Cryst., 23, 617-623.
7. Dollase, W.A. & Baur, W.H. (1976): The superstructure of meteoritic low tridymite solved by computer simulation. Am. Mineral., 61, 971-978.
8. Flörke, O.W. & Langer, K. (1972): Hydrothermal recrystallization and transformation of tridymite. Contrib. Mineral. Petrol., 26, 221-230.
9. Fyfe, C.A., Yi Feng, Grondey, H. (1993): Evaluation of chemical shift-structure correlations from a combination of x-ray diffraction and 2D MAS NMR data for highly siliceous zeolite frameworks. Microporous Materials, 1, 393-400.
10. Graetsch, H. & Flörke, O.W. (1991): X-ray powder diffraction and phase relationship of tridymite modifications. Z. Kristallogr., 195, 31-48.
11. 29Si MAS-NMR study on some non-crystalline silica minerals. J. Non-Cryst. Solids, 119, 173-180.
12. Gibbs, R.E. (1927): The polymorphism of silicon dioxide and the structure of tridymite. Proc. R. Soc., A113, 351-368.
13. Hoffmann, W. (1967): Gitterkonstanten und Raumgruppe von Tridymit bei 20°C. Naturwiss., 54, 114.
14. Hoffmann, W., Kockmeyer, M., Löns, J., Vach, Chr. (1983): The transformation of monoclinic lowtridymite MC to a phase with an incommensurate superstructure. Fortschr. Mineral., 61, 96-98.
15. Kato, K. & Nukui, A. (1976): Die Kristallstruktur des monoklinen Tief-Tridymits. Acta Cryst., B32, 2486-2491.
16. Kihara, K. (1977): An orthorhombic superstructure of tridymite existing between about 105 and 180°C. Z. Kristallogr., 146, 185-203.
17. Kihara, K., Matsumoto, T., Imamura, M. (1986): Structural change of orthorhombic-I tridymite with temperature: a study based on second order thermal-vibrational parameters. Z. Kristallogr., 177, 27-38.
18. Konnert, J.H. & Appleman, D.E. (1978): The crystal structure of low tridymite. Acta Cryst., B34, 391-401.
19. Korekawa, M. (1967): Theorie der Satellitenreflexe. Habilitationsschrift, Ludwig Maximilians Universität München.
20. Liebau, F. (1985): Structural chemistry of silicates. p. 30, Springer Verlag Berlin.
21. Löns, J. & Hoffmann, W. (1987): Zur Kristallstruktur der inkommensurablen Raumtemperaturphase des Tridymits. Z. Kristallogr., 178, 141-143.
22. Mackay, A.L. (1953): A statistical treatment of super-lattice reflexions. Acta Cryst., 6, 214-214.
23. Nukui, A. & Flörke, O.W. (1987): Three tridymite structural modifications and cristobalite intergrown in one crystal. Am. Mineral., 72, 167-169.
24. Nukui, A. & Nakazawa, H. (1980): Polymorphism in tridymite. J. Mineral. Soc. Japan, 14, spec. vol. 2, 241-244 (in Japanese).
25. Nukui, A., Nakazawa, H., Akao, M. (1978): Thermal changes in monoclinic tridymite. Am. Mineral., 63, 1252-1259.
26. Nukui, A., Yamamoto, A., Nakazawa, H. (1979): Nonintegral phase in tridymite. Cowley, J.M., Cohen, J.B., Salamon, M.B., Wuensch, B.J. (eds.): Modulated structures. American Institute of Physics Conference Proceedings no. 53, 327-329.
27. Sheldrick, G.M. (1990): SHELXTL (Program for crystal structure determination).
28. Smith, J.V. & Blackwell, C.S. (1983): Nuclear magnetic resonance of silica polymorphs. Nature, 303, 223-225.
29. 29Si MAS NMR investigation. Am. Mineral., 78, 241-244.
30. 29Si MAS NMR - modulated structures and structural phase transitions. Phys. Chem. Minerals, 22, 30-40.