High-resolution 29Si solid-state NMR study of silicon functionality distribution on the surface of silicas

Magnetic Resonance Imaging

Volumn 14, Issue 7-8, 1996, Pages 911-913

  Luhmer, M ^a   D'Espinose, J B ^a   Hommel, H ^a   Legrand, A P ^a  

^a PSL RESEARCH UNIVERSITY   (France)

Author keywords

29Si NMR; Mesoporous silica

Indexed keywords

SILICON; SILICON DIOXIDE; ISOTOPE;

CONFERENCE PAPER; LIQUID CRYSTAL; MOLECULAR INTERACTION; NUCLEAR MAGNETIC RESONANCE; PRIORITY JOURNAL; STATISTICAL ANALYSIS; ARTICLE; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; POROSITY;

ISOTOPES; MAGNETIC RESONANCE SPECTROSCOPY; POROSITY; SILICON; SILICON DIOXIDE;

EID: 0029658293     PISSN: 0730725X     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0730-725X(96)00180-4     Document Type: Conference Paper

References (5)

1. 29Si solid state NMR. J. Non-Cryst. Solids 155:122-130; 1993.
2. 2. Kresge, C.T.; Leonowicz, M.E.; Roth, W.J.; Vartulli, J.C.; Beck, J.S. Ordered mesoporous molecular sieves synthesised by a liquid-crystal template mechanism. Nature 359:710-712; 1992.
3. 3. Beck, J.S.; Vartulli, J.C.; Roth, W.J.; Leonowicz, M.E.; Kresge, C.T.; Schmitt, K.D.; Chu, C.T-W.; Olson, D.H.; Sheppard, E.W.; McCullen, S.B.; Higgins, J.B.; Schlenker, J.L. A new family of mesoporous molecular sieves prepared with liquid crystal templates. J. Am. Chem. Soc. 114:10834-10843, 1992.
4. 29Si CP/MAS solid-state NMR spectroscopy. Molec. Phys. 71:769-780, 1990.
5. 5. Bronnimann, C.E.; Zeigler, R.C.; Maciel, G.E. Proton NMR study of dehydration of the silica gel surface. J. Am. Chem. Soc. 110:2023-2026, 1988.