Synthesis, Structure, and Redox Chemistry of Heteropolymetallic Carbon Complexes with MC2M’, MC4M’, and MC4M’C4M Linkages. Transmetalations of Lithiocarbon Complexes (η5-C5Me5)Re(NO)(PPh3)(C≡CLi) and (η5-C5Me5)Re(NO)(PPh3)(C≡CC≡CLi)

Journal of the American Chemical Society

Volumn 117, Issue 48, 1995, Pages 11922-11931

  Weng, Weiqing ^a   Bartik, Tamás ^a   Brady, Monika ^a   Bartik, Berit ^a   Ramsden, James A ^a   Arif, Atta M ^a   Gladysz, J A ^a  

^a UNIVERSITY OF UTAH   (United States)

Author keywords

[No Author keywords available]

Indexed keywords

COMPLEXATION; REDOX REACTIONS; STRUCTURE (COMPOSITION); SYNTHESIS (CHEMICAL);

ELECTRON OXIDATION; HETEROPOLYMETALLIC CARBON COMPLEXES; LITHIOCARBON COMPLEXES; TRANSMETALATIONS;

RHENIUM COMPOUNDS;

EID: 0029638225     PISSN: 00027863     EISSN: 15205126     Source Type: Journal    
DOI: 10.1021/ja00153a014     Document Type: Article

References (69)

1. Lang, H. Angew. Chem., Int. Ed. Engl. 1994, 33, 547.
2. Beck, W.; Niemer, B.; Wieser, M. Angew. Chem., Int. Ed. Engl. 1993, 32, 923.
3. Browser, J.R. Adv. Organomet. Chem. 1994, 36, 51.
4. Bradley, J.S. Adv. Organomet. Chem. 1983, 22, 1.
5. Diederich, F.; Rubin, Y.; Chapman, O.L.; Goroff, N.S. Helv. Chim. Acta 1994, 77, 1441.
6. Morton, M.S.; Selegue, J.P. J. Am. Chem. Soc. 1995, 117, 7005.
7. Somorjai, G.A. Introduction to Surface Chemistry and Catalysis; Wiley: New York, 1994; Chapter 7, 8, 2-7. 8, 3.
8. Akita, M.; Moro-oka, Y. Bull. Chem. Soc. Jpn. 1995, 68, 420.
9. Sonogashira, K.; Kataoka, S.; Takahashi, S.; Hagihara, N. J. Organomet. Chem. 1978, 160, 319.
10. Wong, A.; Kang, P.C.W.; Tagge, C.D.; Leon, D.R. Organometallics 1990, 9, 1992.
11. Fyfe, H.B.; Mlekuz, M.; Zargarian, D.; Taylor, N.J.; Marder, T.B. J. Chem. Soc., Chem. Commun. 1991, 188.
12. Stang, P.J.; Tykwinski, R. J. Am. Chem. Soc. 1992, 114, 4411.
13. Crescenzi, R.; Sterzo, C.L. Organometallics 1992, 11, 4301.
14. Rappert, T.; Nümberg, O.; Werner, H. Organometallics 1993, 12, 1359.
15. Le Narvor, N.; Lapinte, C. J. Chem. Soc., Chem. Commun. 1993, 357.
16. Bruce, M.I.; Hinterding, P.; Tiekink, E.R.T.; Skelton, B.W.; White, A.H. J. Organomet. Chem. 1993, 450, 209.
17. Le Narvor, N.; Toupet, L.; Lapinte, C. J. Am. Chem. Soc. 1995, 117, 7129.
18. Kim, P.J.; Masai, H.; Sonogahira, K.; Hagihara, N. lnorg. Nucl. Chem. Lett. 1970, 181.
19. Lagow, R.J.; Kampa, J.J.; Wei, H.-C.; Battle, S.L.; Genge, J.W.; Laude, D.A.; Harper, C.J.; Bau, R.; Stevens, R.C.; Haw, J.F.; Munson, E. Science, 1995, 267, 362.
20. Ramsden, J.A.; Weng, W.; Gladysz, J.A. Organometallics 1992, 11, 3635.
21. Ramsden, J.A.; Weng, W.; Arif, A.M.; Gladysz, J.A. J. Am. Chem. Soc. 1992, 114, 5890.
22. Weng, W.; Ramsden, J.A.; Arif, A.M.; Gladysz, J.A. J. Am. Chem. Soc. 1993, 115, 3824.
23. Weng, W.; Arif, A.M.; Gladysz, J.A. Angew. Chem., Int. Ed. Engl. 1993, 32, 891.
24. Weng, W.; Bartik, T.; Gladysz, J.A. Angew. Chem., Int. Ed. Engl. 1994, 33, 2199.
25. Zhou, Y.; Seyler, J.W.; Weng, W.; Arif, A.M.; Gladysz, J.A. J. Am. Chem. Soc. 1993, 115, 8509.
26. Seyler, J.W.; Weng, W.; Zhou, Y.; Arif, A.M.; Gladysz, J.A. Organometallics 1993, 12, 3802.
27. Brady, M.; Weng, W.; Gladysz, J.A. J. Chem. Soc., Chem. Commun. 1994, 2655.
28. Bartik, T.; Bartik, B.; Brady, M.; Dembinski, R.; Gladysz, J.A. Submitted for publication.
29. Parker, D.W.; Marsi, M.M.; Gladysz, J.A. J. Organomet. Chem. 1980, 194, C1.
30. Brandsma, L. Preparative Acetylenic Chemistry, 2nd ed.; Elsevier: New York, 1988; p 179.
31. Holmes, A.B.; Jennings-White, C.L.D.; Schulthess, A.H.; Akinde, B.; Walton, D.R.M. J. Chem. Soc., Chem. Commun. 1979, 840.
32. Zweifel, G.; Rajagopalan, S. J. Am. Chem. Soc. 1985, 107, 700.
33. Peng, T.-S.; Winter, C.H.; Gladysz, J.A. lnorg. Chem. 1994, 33, 2534.
34. Mann, F.G. J. Chem. Soc. 1935, 1549.
35. Wilkinson, G. lnorg. Synth. 1968, 11, 99.
36. Kowalczyk, J.J.; Arif, A.M.; Gladysz, J.A. Organometallics 1991, 10, 1079.
37. Eastmond, R.; Johnson, T.R.; Walton, D.R.M. J. Organomet. Chem. 1973, 50, 87.
38. Senn, D.R.; Wong. A.; Patton, A.T.; Marsi, M.; Strouse, C.E.; Gladysz, J.A. J. Am. Chem. Soc. 1988, 110, 6096.
39. Heidrich, J.; Steimann, M.; Appel, M.; Beck, W.; Phillips, J.R.; Trogler, W.C. Organometallics 1990, 9, 1296.
40. Onitsuka, K.; Ogawa, H.; Joh, T.; Takahahi, S.; Yamamoto, Y.; Yamazaki, H. J. Chem. Soc., Dalton Trans. 1991, 1531.
41. de Graaf, W.; Harder, S.; Boersma, J.; van Koten, G.; Kanters, J.A. J. Organomet. Chem. 1988, 358, 545.
42. van der Voort, E.; Spek, A.L.; de Graaf, W. Acta Crystallogr. 1987, C43, 2311.
43. Behrens, U.; Hoffmann, K. J. Organomet. Chem. 1977, 129, 273.
44. Yasuda, T.; Kai, Y.; Yasuoka, N.; Kasai, N. Bull. Chem. Soc. Jpn. 1977, 50, 2888.
45. Sandstrom, J. Dynamic NMR Spectroscopy; Academic Press: New York, 1982; Chapter 7.
46. Mew, P.K.T.; Vogtle, F. Angew. Chem., Int. Ed. Engl. 1979, 18, 159.
47. Ogawa, H.; Onitsuka, K.; Joh, T.; Takahashi, S.; Yamamoto, Y.; Yamazaki, H. Organometallics 1988, 7, 2257.
48. Creutz, C. Prog. lnorg. Chem. 1983, 30, 1.
49. Sponsler, M.B. Organometallics 1995, 14, 1920 and references therein.
50. Calvin, G.; Coates, G.E. J. Chem. Soc. 1960, 2008.
51. Davey, A.P.; Cardin, D.J.; Byrne, H.J.; Blau, W. In Organic Molecules of Nonlinear Optics and Photonics; Messier, J., Kajzar, F., Prasad, P., Eds.; Kluwer: Boston, 1991; pp 391—402.
52. Eastmond, R.; Johnson, T.R.; Walton, D.R.M. Tetrahedron 1972, 28, 4601.
53. Yamaguchi, M.; Park, H.-J.; Hirama, M.; Torisu, K.; Nakamura, S.; Minami, T.; Nishihara, H.; Hiraoka, T. Bull. Chem. Soc. Jpn. 1994, 67, 1717.
54. Walton, D.R.M.; Waugh, F. J. Organomet. Chem. 1972, 37, 45.
55. Since yields are a sensitive function of conditions, full details of our version of the original synthesis are given in this paper.
56. Ustynyuk, N.A.; Vinogradova, V.N.; Krautsov, D.N.; Oprunenko, Y.F.; Piven, V.A. Metallorg. Khim. 1988, 1, 884.
57. Chem. Abstr. 1989, 111, 233074c.
58. Muller, T.E.; Choi, S.W.-K.; Mingos, D.M.P.; Murphy, D.; Williams, D.J.; Yam, V.W.-W. J. Organomet. Chem. 1994, 484, 209.
59. Gamasa, M.P.; Gimeno, J.; Godefroy, I.; Lastra, E.; Martin-Vaca, B.M.; Garcia-Granda, S.; Gutierrez-Rodriguez, A. J. Chem. Soc., Dalton Trans. 1995, 1901.
60. Gleiter, R.; Schafer, W. In Supplement C2: The Chemistry of Triple-Bonded Functional Groups; Patai, S., Ed.; Wiley: New York, 1994; pp 157–180.
61. Lichtenberger, D.L.; Rai-Chaudhuri, A.R.; Seidel, M.J.; Gladysz, J.A.; Agbossou, S.K.; Igau, A.; Winter, C.H. Organometallics 1991, 10, 1355.
62. Lichtenberger, D.L.; Gruhn, N.E.; Rai-Chaudhuri, A.; Renshaw, S.K.; Gladysz, J.A.; Seyler, J.; Igau, A. Submitted for publication.
63. Lichtenberger, D.L.; Renshaw, S.K.; Bullock, R.M. J. Am. Chem. Soc. 1993, 115, 3276.
64. Lichtenberger, D.L.; Renshaw, S.K.; Wong, A.; Tagge, C.D. Organometallics 1993, 12, 3522, and references therein.
65. Patton, A.T.; Strouse, C.E.; Knobler, C.B.; Gladysz, J.A. J. Am. Chem. Soc. 1983, 105, 5804.
66. Hölzl, F.; Wrackmeyer, B. J. Organomet. Chem. 1979, 179, 397.
67. Kamienska-Trela, K. Org. Magn. Reson. 1980, 14, 398.
68. Frenz, B.A. The Enraf-Nonius CAD 4 SDP—A Real-time System for Concurrent X-ray Data Collection and Crystal Structure Determination. In Computing and Crystallography; Schenk, H., Olthof-Hazelkamp, R., van Konigsveld, H., Bassi, G.C., Eds.; Delft University Press: Delft, Holland, 1978; pp 64–71.
69. Cromer, D.T.; Waber, J.T. In International Tables for X-ray Crystallography; Ibers, J.A., Hamilton, W.C., Eds.; Kynoch: Birmingham, England, 1974; Vol. IV, Tables 2. 2B and 2, 3, 1.