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Tetrahedron Letters

Volumn 36, Issue 31, 1995, Pages 5595-5598

Generation of chiral (η5-indenyl)2(η3-allyl)Ti complex and its highly enantioselective reaction with carbonyl compounds

(3) Urabe, Hirokazu a Yoshikawa, Kaoru a Sato, Fumie a

a TOKYO INSTITUTE OF TECHNOLOGY (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

ALLYL COMPOUND; LIGAND; TITANIUM;

ARTICLE; CHEMICAL REACTION; CHEMICAL STRUCTURE; COMPLEX FORMATION; ENANTIOMER; STEREOSPECIFICITY; SYNTHESIS;

EID: 0029115053 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/00404-0399(50)1070X- Document Type: Article

Times cited : (16)

References (26)

1
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2
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3
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4
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5
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6
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- Regio-and stereo-selection reaction of 1,3-dialkyl-substituted allyl anions with aldehydes via?3-allyltitanium compounds
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7
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8
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9
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- For recent reports on preparation and application of chiral bis-cyclopentadienyltitanium complexes, see:
- (1992) Organometallics , vol.11 , pp. 3600
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10
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11
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12
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13
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14
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15
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17
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18
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19
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20
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21
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- Alternative methods for the generation of 2 from 1 are also described in this reference and ref 6
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22
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23
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- n-PrMgCl may be used, but i-BuMgCl could not. This observation is in stark contrast to the successful preparation of 2 from 1 with i-BuMgCl. See ref 10.

24
- 84913985135
- 1H NMR analysis of a crude sample revealed the presence of the title compound (threo/erythro = 76:24) in quantitative yield. Chromatography on silica gel afforded the title threo compound (4.7 mg, 67%, or 88% based on the isomeric ratio), threo/erythro = 95:5) and the erythro isomer (1.9 mg, 24% (or quantitative [[Truncated]]

25
- 84913985134
- 2OMTPA of 17b prepared from 11b are quite similar to those of 17a, indicating the absolute stereochemistry of 11b should be the same as that of 11a.

26
- 84913985133
- For instance, authentic samples of 13 were prepared by the following reactions with known stereochemical outcome (Gao, Y.; Urabe, H.; Sato, F. J. Org. Chem. 1994, 59, 5521).

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.