SCOPUS 정보 검색 플랫폼

Volumn 36, Issue 39, 1995, Pages 7115-7118

Activation of carboxylic acids by pyrocarbonates. Application of di-tert-butyl pyrocarbonate as condensing reagent in the synthesis of amides of protected amino acids and peptides

(1) Pozdnev, Vladimir F a

a INSTITUTE OF BIOMEDICAL CHEMISTRY (Russian Federation)

Author keywords

[No Author keywords available]

Indexed keywords

AMINO ACID DERIVATIVE; CARBOXYLIC ACID DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; ENANTIOMER; HIGH PERFORMANCE LIQUID CHROMATOGRAPHY; METHODOLOGY; PEPTIDE SYNTHESIS;

EID: 0029076025 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/0040-4039(95)01412-B Document Type: Article

Times cited : (74)

References (14)

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4
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- Convenient synthesis of N-protected amino acid amides.
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5
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- 4 the solution was dried, the solvent was evaporated and the product was triturated with ether. In another variant the reaction mixture was diluted with water (30–40 ml), stirred until crystallization was completed, a residue was then collected by filtration, washed by water, dried and recrystallized as necessary.

6
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7
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- 4, flow rate 1ml/min., UV detection at 254 nm., retention time L,D-form:13.03 min., L,L-form: 15.05 min.

8
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- Miyazawa¹ Donkai² Yamada³ Kuwata⁴

9
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- (1993) J. Am. Chem. Soc. , vol.115 , pp. 4397-4398
- Carpino¹

10
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- (1993) Int. J. Peptide Protein Res. , vol.43 , pp. 53-57
- Galaverna¹ Corradini² Dossena³ Marchelli⁴

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- (1970) Bull. Chem. Soc. Jap. , vol.43 , pp. 1564-1567
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- Smith¹ Bergmann²

14
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- D −47.4° (c 1, EtOH).

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.