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Volumn 36, Issue 49, 1995, Pages 8961-8964

Synthesis of N-BOC-D-diphenylalanine from L-serine methyl ester hydrochloride

Author keywords

[No Author keywords available]

Indexed keywords

DIPEPTIDE; PHENYLALANINE DERIVATIVE;

EID: 0028877347     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(95)01983-O     Document Type: Article
Times cited : (49)

References (44)
  • 6
    • 84915374926 scopus 로고    scopus 로고
    • Beylin V., Chen H.G., Goel O.P., Topliss J.G. US patent 1993 5,198.548.
  • 9
    • 84915374925 scopus 로고    scopus 로고
    • Czarniecki M.F. US Patent 1988, 4,766,109.
  • 24
    • 84915374924 scopus 로고    scopus 로고
    • US patent application has been filed. Sibi M.P: Deshpande P.K., La Loggia A.J., 08/410,861.
  • 25
    • 84915374923 scopus 로고    scopus 로고
    • 2. All new compounds prepared showed physical, spectral (IR, NMR, and MS), and analytical data consistent with their structure
  • 26
    • 84915374922 scopus 로고    scopus 로고
    • Sibi M.P., Harris B., Renhowe P.A., Christensen J.W., Rutherford D., Li B., Lu J. Org. Synth. submitted for publication.
  • 32
    • 84993865244 scopus 로고
    • Reactions of Sodiurn Borohydride in Acidic Media; IV. Reduction of Diarylmethanols and Triarylmethanols in Trifluoroacetic Acid1-3
    • (1977) Synthesis , pp. 172
    • Gribble1    Leese2    Evans3
  • 33
    • 0001129082 scopus 로고
    • 3Less than 1% of the Birch reduction product was observed. For examples of deoxygenation using Li/NH see:
    • (1975) J. Org. Chem. , vol.40 , pp. 3151
    • Small1    Minnella2
  • 37
    • 84915374921 scopus 로고    scopus 로고
    • 3 (270 MHz), δ 3.96 (d, J=10.3 Hz, 1H), 4.08 (dd, J=8.8, 5.9 Hz. 1H), 4.39 (app. t. J=8.8, 8.1 Hz, 1H). 4.56-4.65 (m, 1H), 5.20 (bs, 1H), 7.15-7.45 (m. 10H): [[Truncated]]
  • 39
    • 84915374920 scopus 로고    scopus 로고
    • %ee was determined by HPLC using a Chiralcel OD column.
  • 41
    • 84915374919 scopus 로고    scopus 로고
    • + column.
  • 43
    • 84915374918 scopus 로고    scopus 로고
    • The preparation of other diaryl amino acids is described in the patent application of this process, see: reference 10.
  • 44
    • 84915374917 scopus 로고    scopus 로고
    • The utility of oxazolidinone 4 in aldol, alkylation, and Diels-Alder reactions is described in the next letter in this issue.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.