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Volumn 36, Issue 47, 1995, Pages 8681-8684

N-Benzyltriflamide: A generally useful mitsunobu reagent for amine synthesis

Author keywords

[No Author keywords available]

Indexed keywords

AMINE;

EID: 0028868443     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(95)01792-G     Document Type: Article
Times cited : (23)

References (23)
  • 3
    • 0028587018 scopus 로고
    • Improved Synthesis of ChiralN-Protected Allylic Amines
    • and for recent contributions to this area, see
    • (1994) Synthesis , pp. 1463
    • Wei1    Knaus2
  • 5
    • 0027763642 scopus 로고
    • Silver iodide mediated amination reaction of allylic chlorides with lithium bis(trimethylsilyl)amide: a new synthetic method of N,N-disilylallylamines via lithium amide argentates
    • (1993) The Journal of Organic Chemistry , vol.58 , pp. 7440
    • Murat1    Yamamoto2    Kondo3    Kato4
  • 8
    • 0028205262 scopus 로고
    • An Improved Procedure for the Preparation of the Garner Aldehyde and Its Use for the Synthesis ofN-Protected 1-Halo-2-(R)-amino-3-butenes
    • See. for example
    • (1994) Synthesis , pp. 31
    • Mckillop1    Taylor2    Watson3    Lewis4
  • 9
    • 85077634689 scopus 로고
    • The Use of Diethyl Azodicarboxylate and Triphenylphosphine in Synthesis and Transformation of Natural Products
    • (1981) Synthesis , pp. 1
    • Mitsunobu1
  • 16
    • 0003068509 scopus 로고
    • N,N,N',N'-Tetramethylazodicarboxamide(TMAD), A New Versatile Reagent for Mitsunobu Reaction. Its Application to Synthesis of Secondary Amines.
    • (1994) Chemistry Letters , pp. 539
    • Tsunoda1    Otsuka2    Yamamiya3    Itô4
  • 17
    • 84915389313 scopus 로고    scopus 로고
    • 1.
  • 21
    • 84915389312 scopus 로고    scopus 로고
    • 1) for 24h then evaporated and the residue separated by column chromatography. Tnbutylphosphine can be used in place of triphenylphosphine; preliminary experiments indicate that such reactions are slightly faster and at least as efficient.
  • 22
    • 84915389311 scopus 로고    scopus 로고
    • The derived chiral N-benzyl tnflamide was compared with similarly prepared racemic material using hplc which indicated an optical purity of 〉 95%.
  • 23
    • 84915389310 scopus 로고    scopus 로고
    • Barks J.M., Kuijpers A.J. and Knight D.W. unpublished observations.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.