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Tetrahedron Letters

Volumn 36, Issue 44, 1995, Pages 8123-8126

Reductive electrophilic substitution of phthalans and ring expansion to isochroman derivatives

(5) Azzena, Ugo a Demartis, Salvatore a Fiori, Maria Giovanna a Melloni, Giovanni a Pisano, Luisa a

a UNIVERSITY OF SASSARI (Italy)

Author keywords

[No Author keywords available]

Indexed keywords

ISOCHROMAN DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; REACTION ANALYSIS;

EID: 0028860818 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/0040-4039(95)01692-B Document Type: Article

Times cited : (32)

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- 2 quenching was performed by bubbling the gaseous electrophile into the reaction mixture for 5 min., and work up as above. The crude products were purified by flash-ehromatography.

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- 2. The crude products were purified by flashchromatography.

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- For a recent application of the reductive lithiation procedure to the ring expansion of thiochroman and related systems, see:, and accompanying paper. We thank Prof. T. Cohen for a preprint copy of the manuscripts.
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20
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- Financial support from MURST, Roma (60% and 40% funds) is gratefully acknowledged.

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