SCOPUS 정보 검색 플랫폼

Volumn 35, Issue 20, 1994, Pages 3391-3394

Simple synthesis of a C2 symmetric vicinal diamine: Highly diastereoselective Grignard addition to a chiral bis-imine

Author keywords

[No Author keywords available]

Indexed keywords

ETHYLENEDIAMINE DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; NUCLEAR MAGNETIC RESONANCE; REACTION ANALYSIS; STEREOCHEMISTRY;

EID: 0028302737 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4039(00)76916-4 Document Type: Article

Times cited : (96)

References (19)

2
- 0002991196
- Asymmetric Synthesis Utilizing External Chiral Ligands
- (1990) Synthesis , pp. 541
- Tomioka¹

5
- 0027494604
- (1993) Tetrahedron , vol.49 , pp. 9735
- Nakajima¹ Tomioka² Koga³

7
- 0011231534
- and references therein
- (1986) J. Org. Chem. , vol.51 , pp. 3635
- Eleveld¹ Hogeveen² Schudde³

9
- 0026075037
- (1991) Tetrahedron Lett. , vol.32 , pp. 5865
- Neumann¹ Rogic² Dunn³

10
- 84912947670
- 2O (100 ml) at −70°C under a nitrogen atmosphere was added by syringe pump over a period of 1h, PhMgCl (60.6 ml of a 2M solution in THF, 0.12 mol). A white precipitate formed immediately, and the mixture was then allowed to warm to room temperature over a period [[Truncated]]

11
- 84912931361
- Crystal data for 7: Orthorhombic, a = 9.095(2), b = 14.403(1), c = 18.997(3) Å, space group P2, 2, 2. R=0.0544 for 1725 observed reflections. Full data deposited with Cambridge Crystallographic Data Centre.

15
- 33749088985
- A similar outcome is seen in reactions of α-amino imines see, Int. Ed. Engl.
- (1991) Angew. Chem. , vol.30 , pp. 103
- Reetz¹ Jaeger² Drewlies³ Hübel⁴

16
- 0000759163
- Other syntheses are longer or involve less readily available starting materials. For the best alternatives see reference 14 and
- (1992) J. Org. Chem. , vol.57 , pp. 6653
- Nantz¹ Lee² Bender³ Roohi⁴

18
- 84985265311
- Studien zum Vorgang der Wasserstoffübertragung, 73. Die Reduktion prochiraler Alkyl(aryl)ketone zu Carbinolen und Pinakolen mit Alkaliamalgamen
- Simpler analogues of 7 and 8 having R = H, are also very readily prepared, see
- (1984) Liebigs Annalen der Chemie , pp. 1240
- Horner¹ Dickerhof²

19
- 84983950393
- Diazadienes as Controlling Ligands in Catalysis, 51). Synthesis of Chiral Diazadienes R* – N = CR' – CR' = N – R*
- (1984) Chemische Berichte , vol.117 , pp. 694
- Dieck¹ Dietrich²

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.