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Volumn 5, Issue 3, 1994, Pages 321-324

Resolution of a cyclopalladated complex containing an asymmetric metallated carbon atom

Author keywords

[No Author keywords available]

Indexed keywords

PALLADIUM COMPLEX;

ARTICLE; DRUG PURIFICATION; ENANTIOMER; NUCLEAR MAGNETIC RESONANCE; PRIORITY JOURNAL;

EID: 0028294561 PISSN: 09574166 EISSN: 1362511X Source Type: Journal
DOI: 10.1016/S0957-4166(00)86196-0 Document Type: Article

Times cited : (33)

References (24)

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- Pfeffer¹

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- During the course of this work a related study was disclosed, Chem. Abstr. 117 1992 26762j
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- Dunina¹ Golovan² Kazakova³ Potapov⁴ Beletskaya⁵

18
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- 8-Ethylquinoline derivatives were synthesised according to
- (1945) J. Am. Chem. Soc. , vol.67 , pp. 86
- Campbell¹ Schaffner²

19
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- 1a and 1b were synthesised according to
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- Sokolov¹ Sorokina² Troitskaya³ Solovieva⁴ Reutov⁵

22
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- 2);2.55 (m, 1H, NH); 3.58 & 3.72 (2m, 2H, CHN & NH); 3.98 ( q, 1H, PdCHMe); 7.14 (dd, 1H, [[Truncated]]

23
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- Curiously, although a whole host of similar complexes (with other amino acids and amino alcohols) of 1a and 1b are known, leucine derivatives give the best results for the resolution process (J. Dupont, R. Konrath, M. Pfeffer, J. Spencer, unpublished observations). However, other more conventional resolution techniques (such as tartaric acid derivatives etc) have not yet been attempted.

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