SCOPUS 정보 검색 플랫폼

Volumn 35, Issue 51, 1994, Pages 9509-9512

Synthesis of N-substituted hydroxyprolinol phosphoramidites for the preparation of combinatorial libraries

Author keywords

[No Author keywords available]

Indexed keywords

OLIGOMER; PHOSPHORAMIDIC ACID DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; METHODOLOGY; REACTION ANALYSIS;

EID: 0028148638 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/0040-4039(94)88498-6 Document Type: Article

Times cited : (33)

References (16)

4
- 0003458038
- Springer-Verlag, New York
- (1984) Principles of Nucleic Acid Structure , pp. 385-431
- Saenger¹

5
- 0027156567
- A similar strategy has been used to prepare 3′-modified oligonucleotides
- (1993) Nucleic Acids Res. , vol.21 , pp. 145-150
- Gamper¹ Reed² Cox³ Virosco⁴ Adams⁵ Gall⁶ Scholler⁷ Meyer⁸

6
- 0026185492
- (1991) Bioconjugate Chem. , vol.2 , pp. 217-225
- Reed¹ Adams² Nelson³ Meyer⁴

7
- 0003463148
- 2nd edition, Wiley, New York
- (1991) Protective Groups in Organic Synthesis , pp. 318
- Greene¹ Wuts²

9
- 33845558546
- (1981) J. Org. Chem. , vol.46 , pp. 2954-2960
- Baker¹ Fritschel² Stille³ Stille⁴

10
- 0003714943
- M.J. Gait, Oxford University Press, New York
- (1984) Oligonucleotide Synthesis: a Practical Approach , pp. 23-34
- Jones¹

11
- 84913010462
- 3) δ 158.74, 145.02, 136.22, 130.09, 128.20, 127.84, 127.71, 126.79, 113.14, 85.97, 72.25, 65.85, 56.68, 55.25, 54.66, 38.45.

13
- 84912991929
- The Fmoc group was cleaved by triethylamine used in the chromatography solvent and by diisopropylamine liberated from the phosphitylating reagent.

14
- 84987487370
- A Simple and Effective Chemical Phosphorylation Procedure for Biomolecules
- (1987) Helvetica Chimica Acta , vol.70 , pp. 175-186
- Bannwarth¹ Trzeciak²

15
- 84912970758
- 3CN (0.1M). Cyanoethyl tetraisopropylphosphorodiamidite added (1.5 eq), followed by diisopropylammonium tetrazolide (0.5 eq). Once the reaction was complete (2–16 h) the solvent was removed and the oil applied to a silica gel column and eluted with a mixture of ethyl acetate/hexanes containing 0.5% triethylamine.

16
- 84912968948
- The purity of the dimers is measured from the peak areas on the HPLC chromatograms. Unreacted dT and protecting group hydrolysis products are not considered impurities.

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