메뉴 건너뛰기
Tetrahedron: Asymmetry
Volumn 5, Issue 1, 1994, Pages 5-8
Synthesis of (R)- and (S)-isopropylidene glycerol
Author keywords

[No Author keywords available]
Indexed keywords

GLYCEROL DERIVATIVE; ISOPROPYLIDENEGLYCEROL; UNCLASSIFIED DRUG;
EID: 0028120770     PISSN: 09574166     EISSN: 1362511X     Source Type: Journal    
DOI: 10.1016/S0957-4166(00)80470-X     Document Type: Article
Times cited : (35)
References (16)
  • 3
    • 84908839347 scopus 로고    scopus 로고
    • M.A. Bertola, H.S. Koger, G.T. Phillips, A.F. Marx and V.P. Claassen EP 244912. 1987, applicant Gist-Brocades N.V./Shell Int.Res.M.B.V.
  • 8
    • 84908839346 scopus 로고    scopus 로고
    • C.J.Sih US pat 4,931,399, 1990.
  • 9
    • 84908839345 scopus 로고    scopus 로고
    • S.Scolastico It. pat. appl. 20665A/88, 1988.
  • 11
    • 84908839344 scopus 로고    scopus 로고
    • 3): δ ppm 8.85 (s, 1 H), 8.2-7.4 (m, 4 H), 4.7-3.7 (m, 5 H), 1.45 (s, 3 H) and 1.4 (s, 3 H).
  • 13
    • 84908839343 scopus 로고    scopus 로고
    • 1H NMR (DMSO): δ ppm 7.8 (m, 1 H), 7.6-7.3 (m, 8 H), 4.4 (m, 2 H), 4.2 (d, 2 H), 4.1 (dd, 1 H), 3.8 (dd, 1 H), 1.6 (d, 3 H), 1.4 (s, 3 H), 1.3 (s. 3 H).
  • 14
    • 84908839342 scopus 로고    scopus 로고
    • Under these conditions the retention times of the methyl phthalates of (S)-1 and (R)-1 were 38.68 and 43.04 minutes respectively.
  • 15
    • 84908839341 scopus 로고    scopus 로고
    • 3): δ ppm 4.2 (m, 1 H), 4.0 (dd, 1 H), 3.8-3.4 (m, 3 H), 2.4 (br s, 1H), 1.4 (s, 3 H), 1.3 (s, 3 H).
  • 16
    • 84908839340 scopus 로고    scopus 로고
    • (R)- and (S)-1 are produced by Chemi S.p.a., viale F.Testi 117, 20092 Cinisello Balsamo (MI), Italia.

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.