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Volumn 34, Issue 10, 1993, Pages 1625-1628

Synthesis of quinolines and 2,3-dihydro-4(1h)-quinolones. Palladium catalysed reaction of o-iodoanilides with acetylenic carbinols

Author keywords

2,3 dihydro 4(1H) quinolones; acetylenic carbinols.; o lodoanilides; palladium catalysis; quinolines

Indexed keywords

4 QUINOLONE DERIVATIVE; QUINOLINE DERIVATIVE;

EID: 0027464633     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/0040-4039(93)85025-R     Document Type: Article
Times cited : (67)

References (34)
  • 17
    • 0000061873 scopus 로고
    • A Novel Synthesis of Cyclic Imides and Quinolone by Use of PalIadium Catalyzed Carbonylation
    • (1979) HETEROCYCLES , vol.13 , pp. 329
    • Mori1    Chiba2    Ohta3    Ban4
  • 28
    • 0344016065 scopus 로고
    • 158. Studies in the polyene series. Part VI. The preparation of ethinylcarbinols from ??-unsaturated aldehydes
    • The acetylenic carbinols were synthesised by addition of acetylene to the appropriate carbonyl compounds, cf
    • (1942) Journal of the Chemical Society (Resumed) , pp. 733
    • Jones1    McCombie2
  • 30
    • 84914374071 scopus 로고    scopus 로고
    • Alkynols 3 were cyclised by refluxing for 5 h with NaOEt in EtOH.
  • 31
    • 84914374070 scopus 로고    scopus 로고
    • Alkynols 3 were stirred with p-TSA in benzene at room temperature for 48 h.
  • 32
    • 84914374069 scopus 로고    scopus 로고
    • Hydrolysis of compounds 5 was done by stirring with 6M aq. NaOH in 95% EtOH at room temperature for 40 h leading to 3-aryl-1-(2-aminophenyl) prop-2-en-1-ones.
  • 33
    • 84914374068 scopus 로고    scopus 로고
    • 4 at 85°C for 25 min.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.