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Tetrahedron Letters

Volumn 34, Issue 7, 1993, Pages 1167-1170

Highly enantioselective reduction of meso-1,2-dicarboxylic anhydrides

(3) Matsuki, Kenji a Inoue, Hirozumi a Takeda, Mikio a

a MITSUBISHI TANABE PHARMA CORPORATION (Japan)

Author keywords

[No Author keywords available]

Indexed keywords

LACTONE DERIVATIVE;

ARTICLE; PRIORITY JOURNAL; REACTION ANALYSIS; SYNTHESIS;

EID: 0027447594 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4039(00)77518-6 Document Type: Article

Times cited : (66)

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19
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- 84.5%e.e. This value was determined by HPLC analysis using a 4.6 × 150mm CHIRALCEL OB-H (DAICEL Chemical Industries, Ltd.) and the mobile phase composed of n-hexane and ethanol in a ratio of 250:1 (v/v). The flow rate was maintained at 1.0 ml/min, and the procedure was carried out at ambient temperature. The effluent was monitored at 210nm. The retention time of (+)-isomer was 37.6 min. and (−)-isomer was 45.3min.

20
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