Correlation of Structure, Mobility, and Morphological Information in Heterogeneous Polymer Materials by Two-Dimensional Wideline-Separation NMR Spectroscopy

Macromolecules

Volumn 25, Issue 12, 1992, Pages 3273-3277

  Schmidt Rohr, K R ^a   Clause, J ^a   Spiess, H W ^a  

^a MAX PLANCK INSTITUTE FOR POLYMER RESEARCH   (Germany)

Author keywords

[No Author keywords available]

Indexed keywords

BLOCK COPOLYMERS; CORRELATION METHODS; DYNAMICS; MOLECULAR STRUCTURE; MORPHOLOGY; NUCLEAR MAGNETIC RESONANCE; POLARIZATION; POLYMERIC GLASS; RADIOFREQUENCY SPECTROSCOPY;

CROSS POLARIZATION; MOLECULAR DYNAMICS; SEGMENTAL MOBILITY; SPIN DIFFUSION; WIDELINE SEPARATION (WISE);

ORGANIC POLYMERS;

EID: 0027115080     PISSN: 00249297     EISSN: 15205835     Source Type: Journal    
DOI: 10.1021/ma00038a037     Document Type: Article

References (35)

1. Krevelen, D. W. Properties of Polymers; Elsevier: Amsterdam, 1976.
2. Utracki, L. A. Polymer Alloys and Blends; Hanser: Munich, 1989.
3. Quirk, R. P. In Block Copolymers; Allen, G., Bevington, J. C., Aggarwal, S., Eds.; Comprehensive Polymer Science, 7; Pergamon Press: Oxford, U.K., 1989; p 285.
4. Schmidt-Rohr, K.; Spiess, H. W. Phys. Reo. Lett. 1991, 66, 3020.
5. Schaefer, D.; Spiess, H. W.; Suter, U. W.; Fleming, W. W. Macromolecules 1990, 23, 3431.
6. Zemke, K.; Chmelka, B. C.; Schmidt-Rohr, K.; Spiess, H. W. Macromolecules 1991, 24, 6874.
7. Komoroski, R. A., Ed. High Resolution NMR Spectroscopy of Synthetic Polymers in Bulk; VCH Publishers: Deerfield Beach, FL, 1986.
8. Schnauss, W.; Pujara, F.; Hartmann, K.; Sillescu, H. Chem. Phys. Lett. 1990, 166, 381.
9. Wunderlich, B.; Möller, M.; Grebowicz, J.; Bauer, H. Conformational Motion and Disorder in Low and High Molecular Mass Crystals. Adv. Polym. Sci. 1988, 87,1.
10. Spiess, H. W. Deuteron NMR—A New Tool for Studying Chain Mobility and Orientation in Polymers. Adv. Polym. Sci. 1985, 66, 23.
11. Munowitz, M. G.; Aue, Griffin, R. G. J. Chem. Phys. 1982, 77, 1686.
12. Schaefer, J.; Stejskal, E. O.; McKay, R. A.; Dixon, W. T.; Cais, R. E. Macromolecules 1984,17,1107.
13. Caravatti, P.; Braunschweiler, L.; Ernst, R. R. Chem. Phys. Lett. 1983,100, 305.
14. Ernst, R. R.; Bodenhausen, G.; Wokaun, A. Principles of Nuclear Magnetic Resonance in One and Two Dimensions; Clarendon Press: Oxford, U.K., 1987.
15. Hartmann, S. R.; Hahn, E. L. Phys. Reo. 1962, 128, 2042.
16. Pines, A.; Gibby, M. G.; Waugh, J. S. J. Chem. Phys. 1973, 59, 569.
17. Hagemeyer, A.; Schmidt-Rohr, K.; Spiess, H. W. Ado. Magn. Reson. 1989,13, 85.
18. Dixon, W. T. J. Magn. Reson. 1980, 44, 220.
19. Dixon, W. T. J. Chem. Phys. 1982, 77, 1800.
20. Saam, J. C.; Gordon, D. J.; Lindsey, S. Macromolecules 1970, 3, 1.
21. Gerharz, B.; Fytas, G.; Fischer, E. W. Polym. Commun. 1991, 32, 469.
22. Caravatti, P.; Neuenschwander, P.; Ernst, R. R. Macromolecules 1985, 18, 119.
23. Caravatti, P.; Neuenschwander, P.; Ernst, R. R. Macromolecules 1986, 19, 1889.
24. Chu, C. W.; Dickinson, L. C.; Chien, C. W. J. Appl. Polym. Sci. 1990, 41, 2311.
25. Mirau, P. A.; Bovey, F. A. Macromolecules 1990, 23, 4548.
26. Bank, M.; Leffmgwell, J.; Thies, C. Macromolecules 1971, 4, 43.
27. Egger, N.; Schmidt-Rohr, K.; Blümich, B.; Domke, W.-D.; Stapp, B. J. Appl. Polym. Sci., in press. Schmidt-Rohr, K. Diploma Thesis, Mainz, 1989.
28. Miller, J. B.; McGrath, K. J.; Roland, C. M.; Trask, C. A.; Garroway, A. N. Macromolecules 1990, 23, 4543.
29. Crank, J. The Mathematics of Diffusion, 2nd ed.; Clarendon Press: Oxford, U.K., 1975.
30. Schmidt-Rohr, K. Ph.D. Thesis, Mainz, 1991.
31. Clause, J.; Schmidt-Rohr, K.; Spiess, H. W. To be published.
32. Schmidt-Rohr, K.; Spiegel, S.; Spiess, H.W. Unpublished results.
33. Cheung, T. T. P.; Gerstein, B. C. J. Appl. Phys. 1981, 52, 5517.
34. Spiess, H. W. Colloid Polym. Sci. 1983, 261, 193.
35. Inglefield, P.T.; Amici, R. M.; O'Gara, J. F.; Hung, C.-C.; Jones, A. A. Macromolecules 1983, 16, 1552.