Assignments of solid-state 13C resonances for polymorphs of cortisone acetate using shielding tensor components

Solid State Nuclear Magnetic Resonance

Volumn 1, Issue 2, 1992, Pages 93-101

  Christopher, Elizabeth A ^a   Harris, Robin K ^a   Fletton, Richard A ^b  

^a DURHAM UNIVERSITY   (United Kingdom)

^b GLAXOSMITHKLINE   (United Kingdom)

Author keywords

cortisone acetate; CP MAS spectra; shielding tensor components; spectral assignment; spinning sideband analysis

Indexed keywords

CARBON; CORTISONE; CORTISONE ACETATE; DRUG DERIVATIVE;

ARTICLE; CHEMICAL STRUCTURE; CHEMISTRY; COMPARATIVE STUDY; HYDROGEN BOND; METHODOLOGY; NUCLEAR MAGNETIC RESONANCE SPECTROSCOPY; X RAY CRYSTALLOGRAPHY;

CARBON; CARBON ISOTOPES; COMPARATIVE STUDY; CORTISONE; CRYSTALLOGRAPHY, X-RAY; HYDROGEN BONDING; MAGNETIC RESONANCE SPECTROSCOPY; MOLECULAR STRUCTURE; SUPPORT, NON-U.S. GOV'T;

EID: 0026884040     PISSN: 09262040     EISSN: None     Source Type: Journal    
DOI: 10.1016/0926-2040(92)90021-Z     Document Type: Article

References (19)

1. NMR in rotating solids
2. High-field1H and13C NMR spectroscopy of some corticosteroids and related compounds
3. Structure of modification I of cortisone acetate, 21-acetoxy-17α-hydroxy-4-pregnene-3,11,20-trione, C23H30O6
4. Structure of the acetone solvate of 17α-hydroxy-3,11,20-trioxo-4-pregnen-21-yl acetate (cortisone acetate, modification IVac)
5. Structure of the monohydrate of 17α-hydroxy-3,11,20-trioxo-4-pregnen-21-yl acetate (cortisone acetate, modification Vaq)