Speciation of mercury in human whole blood by capillary gas chromatography with a microwave-induced plasma emission detector system following complexometric extraction and butylation

The Analyst

Volumn 117 3, Issue , 1992, Pages 657-663

  Bulska, Ewa ^a,d   Emteborg, Håkan ^a   Baxter, Douglas C ^a   Frech, Wolfgang ^a   Ellingsen, Dag ^b   Thomassen, Yngvar ^c  

^a UMEÅ UNIVERSITY   (Sweden)

^b TELEMARK HOSPITAL   (Norway)

^c NATIONAL INSTITUTE OF OCCUPATIONAL HEALTH   (Norway)

^d UNIVERSITY OF WARSAW   (Poland)

Author keywords

Capillary gas chromatography; Complexometric extraction; Derivatization; Mercury speciation in human whole blood; Microwave induced plasma atomic emission detector

Indexed keywords

MERCURY;

ARTICLE; ATOMIC ABSORPTION SPECTROMETRY; BLOOD; COMPARATIVE STUDY; ENVIRONMENTAL EXPOSURE; GAS CHROMATOGRAPHY; HUMAN; INSTRUMENTATION; ISOLATION AND PURIFICATION; METHODOLOGY; MICROWAVE RADIATION; REFERENCE VALUE;

CHROMATOGRAPHY, GAS; COMPARATIVE STUDY; ENVIRONMENTAL EXPOSURE; HUMAN; MERCURY; MICROWAVES; REFERENCE VALUES; SPECTROPHOTOMETRY, ATOMIC ABSORPTION; SUPPORT, NON-U.S. GOV'T;

EID: 0026828424     PISSN: 00032654     EISSN: None     Source Type: Journal    
DOI: 10.1039/an9921700657     Document Type: Article

References (36)

1. Weiner, J. A., Nylander, M., Berglund, F., Sci. Total Environ., 1990, 99, 1
2. Druet, P., Bernard, A., Hirsch, F., Weening, J. J., Gengoux, P., Mahieu, P., Birkeland, S., Arch. Toxicol., 1982, 50, 187
3. Siblerud, R. L., Sci. Total Environ., 1990, 99, 23
4. D'Itri, F. M., The Environmental Mercury Problem, CRC Press, Cleveland, OH, 1972, pp. 38–44.
5. Barregård, L., Thomassen, Y., Schütz, A., Marklund, S. L., Sci. Total Environ., 1990, 99, 37
6. Westöö, G., Acta Chem. Scand., 1967, 21, 1790
7. Westöö, G., Acta Chem. Scand., 1968, 22, 2277
8. Westöö, G., Norén, K., Vår Föda, 1967, 10, 138
9. Magos, L., Clarkson, T. W., J. Assoc. Off. Anal. Chem., 1972, 55, 966
10. Chang, S. B., Siew, C., Gruninger, S. E., J. Anal. Toxicol., 1987, 11, 149
11. Cappon, C. J., Smith, J. C., Anal. Chem., 1977, 49, 365
12. Cappon, C. J., Smith, J. C., Bull. Environ. Contam. Toxicol., 1978, 19, 600
13. Goolvard, L., Smith, H., Analyst, 1980, 105, 726
14. O'Reilly, J. E., J. Chromatogr., 1982, 238, 433
15. Hight, S. C., J. Assoc. Off. Anal. Chem., 1987, 70, 667
16. Horvat, M., Byrne, A. R., May, K., Talanta, 1990, 37, 207
17. Iverfeldt, Å., Swedish Environmental Research Institute, Gothenburg, Sweden, 1991, personal communication.
18. Bloom, N., Can. J. Fish. Aquat. Sci., 1989, 46, 1131
19. Brunmark, P., and Skarping, G., Poster No. 8 presented at Analysdagarna, Lund, Sweden, June 17–21, 1990.
20. Bulska, E., Baxter, D. C., Frech, W., Anal. Chim. Acta, 1991, 249, 545
21. Beenakker, C. I. M., Spectrochim. Acta, Part B, 1976, 31, 483
22. Bollo-Kamara, A., Codding, E. G., Spectrochim. Acta, Part B, 1981, 36, 973
23. Cammann, K., Lendero, L., Feuerbacher, H., Ballschmiter, K., Fresenius' Z. Anal. Chem., 1983, 316, 194
24. Emteborg, H., Bulska, E., Frech, W., Baxter, D. C., J. Anal. At. Spectrom., 1992, 7, in the press
25. De, A. K., Khopkar, S. M., and Chalmers, R. A., Solvent Extraction of Metals, Van Nostrand Reinhold, New York, 1970, pp. 141–146.
26. Environmental Analysis using Chromatography Interfaced with Atomic Spectroscopy, eds. Harrison, R. M., and Rapsomanikis, S., Ellis Horwood, Chichester, 1989.
27. Nygren, O., Nilsson, C.-A., J. Anal. At. Spectrom., 1987, 2, 805
28. Carvajal, N. J., Zienius, R. M., J. Chromatogr., 1986, 355, 107
29. Miller, J. C., and Miller, J. N., Statistics for Analytical Chemistry, Ellis Horwood, Chichester, 2nd edn., 1988.
30. Holak, W., J. Assoc. Off. Anal. Chem., 1989, 72, 926
31. Bushee, D. S., Analyst, 1988, 113, 1167
32. Kuba, J., Kicera, L., Plzák, M., and Mráz, J., Coincidence Tables for Atomic Spectrometry, Elsevier, Amsterdam, 1965, pp. 681–684.
33. Horvat, M., May, K., Stoeppler, M., Byrne, A. R., Appl. Organomet. Chem., 1988, 2, 850
34. Brooks, A. G. F., Bailey, E., Snowden, R. T., J. Chromatogr., 1986, 374, 289
35. Olssen, K. B., Sklarew, D. S., Evans, J. C., Spectrochim. Acta, Part B, 1985, 40, 357
36. Quimby, B. D., Sullivan, J. J., Anal. Chem., 1990, 62, 1027