An improved multigram-scale preparation of s-tertbutyl acetothioacetate

Synthetic Communications

Volumn 22, Issue 16, 1992, Pages 2329-2333

  Lápez Alvarado, Pilar ^a   Avendan˜o, Carmen ^a   Meneéndez, J Carlos ^a  

^a UNIVERSIDAD COMPLUTENSE DE MADRID   (Spain)

Author keywords

[No Author keywords available]

Indexed keywords

3 ACETYL 4 TERT BUTYLTHIO 6 METHYL 2 PYRONE; ACETIC ACID DERIVATIVE; PYRAN DERIVATIVE; THIOACETOACETIC ACID S TERT BUTYL ESTER; UNCLASSIFIED DRUG;

ARTICLE; REACTION ANALYSIS; SYNTHESIS;

EID: 0026656371     PISSN: 00397911     EISSN: 15322432     Source Type: Journal    
DOI: 10.1080/00397919208019087     Document Type: Article

References (9)

1. R. J. Clemens, Chem. Rev., 1986, 86, 241.
2. C. M. J. Fox and S. V. Ley, Org. Syntheses, 1987, 66, 108.
3. S. V. Ley and P. R. Woodward, Tetrahedron Lett., 1987, 32, 2431.
4. P. M. Booth, C. M. J. Fox and S. V. Ley, J. Chem. Soc. Perkin Trans. I, 1987, 121.
5. P. M. Booth, H. B. Broughton, M. J. Ford, C. M. J. Fox, S. V. Ley, A. M. Z. Slawin, D. J. Williams and P. R. Woodward, Tetrahedron, 1989, 45, 7565.
6. C. Gesto, E. de la Cuesta, C. Avendano, Synthesis, 1991, 727.
7. For a review on the chemistry of 4H-l, 3-dioxin-4-ones, see: M. Sato, Yakugaku Zasshi, 1988, 108, 805.
8. R. J. Clemens and J. S. Witzeman, J. Am. Chem. Soc., 1989, 111, 2186.
9. Compound 4 is commercially available (Aldrich Chemical Company). Physical and spectral data were identical to those previously described.