SCOPUS 정보 검색 플랫폼

Volumn 33, Issue 19, 1992, Pages 2665-2668

Conversion of allylic alcohols into conjugated dienes

Author keywords

allylic alcohols; dehydration; dienes.; Phosphorus oxychloride

Indexed keywords

ALKENE DERIVATIVE; STYRENE DERIVATIVE;

ARTICLE; PRIORITY JOURNAL; REACTION ANALYSIS; SYNTHESIS;

EID: 0026562880 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4039(00)79052-6 Document Type: Article

Times cited : (10)

References (9)

1
- 0001549538
- For example, see, and references cited therein.
- (1982) J. Am. Chem. Soc. , vol.104 , pp. 7051
- Reich¹ Wollowitz²

3
- 0000390810
- (1984) J. Am. Chem. Soc. , vol.106 , pp. 6690
- Paquette¹ Roberts² Drtina³

4
- 0000340978
- Spring-loaded biradicals. The radical and electron-transfer photochemistry of bridgehead cyclopropyl-substituted 2,3-diazabicyclo[2.2.2]oct-2-enes (DBO's)
- (1985) Journal of the American Chemical Society , vol.107 , pp. 4964
- Engell¹ Keys² Kitamura³

5
- 0001139107
- (1986) J. Am. Chem. Soc. , vol.108 , pp. 3443
- Mehta¹ Murthy² Reddy³ Reddy⁴

8
- 37049083643
- Short synthesis of (�)-bakuchiol via a geranylindium reagent
- (1991) Journal of the Chemical Society, Perkin Transactions 1 , pp. 2395
- Araki¹ Bustugan²

9
- 84918703821
- A typical experimental procedure is as follows: 1-(2, 6-Dimethoxyphenyl)-3-methyl-2-buten-1-ol (1.11g, 5.00 mM) was dissolved in 5 mL of pyridine and 5 mL of dicloromethane and cooled to 0°. Phosphorus oxychloride (0.56mL, 6.0mM) was added via syringe over 15 sec. The reaction mixture was allowed to warm to RT and stir overnight. Work-up by quenching with aqueous sodium bicarbonate and extraction with ether gave, after filtration through silica gel, 0.80g (80%) of trans-1-(2, 6-dimethoxyphenyl)-3-methyl-1, 3-butadiene.

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