SCOPUS 정보 검색 플랫폼

Volumn 33, Issue 16, 1992, Pages 2115-2118

Preparation and cycloadditions of a 4-methoxy-3-oxidopyrylium ylid: a reagent for the synthesis of highly substituted seven-membered rings and tetrahydrofurans

(2) Wender, Paul A a Mascareñas, Jose L a

a STANFORD UNIVERSITY (United States)

Author keywords

[No Author keywords available]

Indexed keywords

FURAN DERIVATIVE; POLYCYCLIC HYDROCARBON; PYRAN DERIVATIVE;

ARTICLE; PRIORITY JOURNAL; REACTION ANALYSIS; SYNTHESIS;

EID: 0026529744 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/0040-4039(92)88154-W Document Type: Article

Times cited : (68)

References (23)

1
- 0025039722
- (1990) J. Am. Chem. Soc. , vol.112 , pp. 4956
- Wender¹ McDonald²

2
- 0001617538
- (1991) J. Org. Chem. , vol.56 , pp. 6267
- Wender¹ Mascareñas²

3
- 0346466427
- For early studies on the intermolecular reactions, see:
- (1952) J. Am. Chem. Soc. , vol.74 , pp. 3959
- Woods¹

4
- 0347096745
- (1958) J. Am. Chem. Soc. , vol.80 , pp. 2526
- Hurd¹ Trofimenko²

5
- 33947466226
- (1959) J. Am. Chem. Soc. , vol.81 , pp. 2430
- Hurd¹ Trofimenko²

6
- 0345835429
- (1959) J. Am. Chem. Soc. , vol.81 , pp. 1684
- Hurd¹ Sims² Trofimenko³

7
- 0347096746
- For the structure of these adducts, see:
- (1977) J. Org. Chem. , vol.42 , pp. 3976
- Volkmann¹ Weeks² Kuhla³ Whipple⁴ Chmurny⁵

8
- 0343246769
- For a study of the intramolecular reaction, see:
- (1983) Tetrahedron Lett. , vol.24 , pp. 1675
- Garst¹ McBride² Douglas³

9
- 0000284306
- For related work on oxidopyrylium ylides, see:
- (1980) J. Org. Chem. , vol.45 , pp. 3359
- Hendrickson¹ Farina²

10
- 37049099771
- The preparation and some reactions of 3-oxidopyrylium
- (1983) Journal of the Chemical Society, Perkin Transactions 1 , pp. 1261
- Sammes¹ Street²

11
- 0037998555
- (1984) J. Chem. Res. (S) , pp. 196
- Sammes¹ Street²

12
- 0001192252
- (1986) Gazz. Chim. Ital. , vol.119 , pp. 109
- Sammes¹

13
- 0016902140
- (1976) Angew. Chem. Int. Ed. Engl. , vol.15 , pp. 1
- Dennis¹ Katritzky² Takeuchi³

14
- 33845184642
- For a recent review of cycloaddition reactions of heteroaromatic six-membered rings see:
- (1989) Chem. Rev. , vol.89 , pp. 827-861
- Katritzky¹ Dennis²

15
- 0345177190
- α-Deoxykojic Acid and Some of Its Derivatives
- (1958) The Journal of Organic Chemistry , pp. 1276
- Hurd¹

16
- 84918684436
- (1958) J. Chem. Soc. , pp. 2558
- Brown¹

17
- 84918666807
- This salt crystallized from EtOAc as a white solid (m.p. 52°C).

18
- 84918706776
- The endo isomer is defined as that in which the olefinic substituent(s) is anti to the oxido-bridge. The stereochemistry of adducts 10 and 11 was deduced from the coupling constant across the positions 1,7.

19
- 84918692498
- All new compounds gave satisfactory NMR and high resolution mass spectra.

20
- 84918656366
- 1H NMR spectrum, which shows a coupling constant of 2.5 Hz between the protons α to the ketones.

21
- 84918676606
- endo), 1.74 (s, 3H).

22
- 84918705063
- endo), 1.54 (s, 3H).

23
- 84918672834
- 3, 300 MHz) of 17: 5.90 (s, 1H), 4.29 (s, 1H), 3.58 (s, 3H), 2.35 (br d, J∼12 Hz, 2H), 1.98 (br s, 2H), 1.84 (br d, J∼9.8 Hz, 1H), 1.5 (m, 5H), 1.12 (m, 2H), 0.99 (br d, J∼9.6 Hz, 1H).

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.