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Tetrahedron Letters

Volumn 33, Issue 49, 1992, Pages 7613-7616

Azinothricin synthetic studies. 1. Efficient asymmetric synthesis of (3R)- and (3S)-piperazic acids

(3) Hale, Karl J a Delisser, Vern M a Manaviazar, Soraya a

a UNIVERSITY COLLEGE LONDON (United Kingdom)

Author keywords

[No Author keywords available]

Indexed keywords

HETEROCYCLIC CARBOXYLIC ACID; PIPERAZIC ACID; PIPERAZINE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; ENANTIOMER; PRIORITY JOURNAL; SYNTHESIS;

EID: 0026495324 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4039(00)60838-9 Document Type: Article

Times cited : (44)

References (21)

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- L-156602
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7
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8
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- For elegant synthetic studies that have culminated in a total synthesis of L-156602 see, Abstract No. 119
- (1989) th ACS National Meeting Miami Beach, Florida, September 10–15
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- Kopka¹

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14
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18
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- 13C NMR spectra. In addition, an analytical sample of this compound gave a satisfactory C, H, and N combustion microanalysis.

19
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- 3 washings with 10% aq. HCl, and extraction with ethyl acetate.

20
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- 1H NMR spectroscopy, and by subsequent chemical conversions.

21
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- 7: C, 61.33; H, 7.21; N, 8.58. Found: C, 61.17; H, 7.36; N, 8.31.(10) m.p. 115–118°C; IR (KBr): 3209, [[Truncated]]

* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.