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Volumn 32, Issue 12, 1991, Pages 1573-1576

Novel method for generation of secondary organozinc reagent: Application to tandem carbon-carbon bond formation reaction of 1,1-dibromoalkane

Author keywords

[No Author keywords available]

Indexed keywords

ALKANE DERIVATIVE;

EID: 0026073043     PISSN: 00404039     EISSN: None     Source Type: Journal    
DOI: 10.1016/S0040-4039(00)74275-4     Document Type: Article
Times cited : (61)

References (25)
  • 11
    • 33845552397 scopus 로고
    • Selective carbon-carbon bond formation via transition metal catalysis. 37. Controlled carbometalation. 16. Novel syntheses of .alpha.,.beta.-unsaturated cyclopentenones via allylzincation of alkynes
    • (1983) Journal of the American Chemical Society , pp. 6761
    • Negishi1    Miller2
  • 20
    • 84918624170 scopus 로고    scopus 로고
    • 2 with 3 equiv of RLi in THF at 0 °C.
  • 21
    • 84918643196 scopus 로고    scopus 로고
    • The temperature −85 °C is not critical in the present reaction. Authors usually use a Neslab-Cryocool CC-80 immersion cooler in performing low temperature reactions.
  • 22
    • 84918629837 scopus 로고    scopus 로고
    • 3ZnLi.
  • 23
    • 84918601227 scopus 로고    scopus 로고
    • 2).
  • 24
    • 84918639823 scopus 로고    scopus 로고
    • 3, the dried organic layers were concentrated in vacuo and the resulting crude mixture was purified with silica gel column chromatography (hexane) to give 1,3-diphenylheptane in 62% yield.


* 이 정보는 Elsevier사의 SCOPUS DB에서 KISTI가 분석하여 추출한 것입니다.