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Tetrahedron Letters

Volumn 31, Issue 3, 1990, Pages 413-416

Highly selective oxidative cross-coupling of substituted 2-naphthols: A convenient approach to unsymmetrical 1,1′-binaphthalene-2,2′-diols

(3) Hovorka, Martin a Günterová, Jana a Závada, Jiří a

a INSTITUTE OF ORGANIC CHEMISTRY AND BIOCHEMISTRY (Czech Republic)

Author keywords

[No Author keywords available]

Indexed keywords

1,1' BINAPHTHYL DERIVATIVE;

ARTICLE; DRUG SYNTHESIS; NONHUMAN; PRIORITY JOURNAL;

EID: 0025174975 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4039(00)94569-6 Document Type: Article

Times cited : (91)

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- 2 (16 ml of 1M solution in methanol) is added dropwise and the heterogeneous reaction mixture is heated as indicated in Table 1. After the completion the reaction mixture is cooled to approx. 10°C and decomposed with 6M HCl. Methanol is taken down on the evaporator and the product filtered (entry 4) or extracted with chloroform. The biaryls are separated by flash chromatography on silicagel.

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