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Tetrahedron Letters

Volumn 31, Issue 6, 1990, Pages 879-882

A new strategy for the enantioselective synthesis of aspidosperma alkaloids: I - Construction of the [ABC]-type tricyclic intermediates.

(2) d'Angelo, Jean a Desmaele, Didier a

a PSL RESEARCH UNIVERSITY (France)

Author keywords

[No Author keywords available]

Indexed keywords

ASPIDOSPERMIDINE DERIVATIVE; UNCLASSIFIED DRUG;

ARTICLE; DRUG STRUCTURE; DRUG SYNTHESIS; INFRARED SPECTROPHOTOMETRY; NONHUMAN; NUCLEAR MAGNETIC RESONANCE; PRIORITY JOURNAL;

ASPIDOSPERMA;

EID: 0025162030 PISSN: 00404039 EISSN: None Source Type: Journal
DOI: 10.1016/S0040-4039(00)94653-7 Document Type: Article

Times cited : (31)

References (30)

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18
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- 3) δ: 8.24 (1H, m) 8.18 (1H, m) 7.74 (2H, d, J = 8.4 Hz) 7.32 (2H, m) 7.24 (2H, d, J = 8.5 Hz) 3.47 (1H, ddd, J = 18.7 4.6 4.6 Hz) 3.18 (1H, ddd, J = 18.7 10.3 5.1 Hz) 2.55 (1H, m) 2.33 (3H, s) 2.26 (1H, m) 1.92 (1H, m) 1.22 (3H, d, 6.9 Hz).

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22
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24
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25
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- 3) δ: 5.27 (1H, s) 3.70 (3H, s) 3.65 (3H, s) 2.5–1.8 (8H, m) 1.10 (3H, s).

26
- 84918612558
- 4: C 62.24 H 7.59, found: C 62.60 H 7.42.

27
- 84918625866
- 3) δ : 7.86 (1H, d, J = 7.8 Hz) 7.30 (2H, d, J = 4.0 Hz) 6.91 (1H, m) 6.06 (1H, broad s) 5.23 (1H, s) 3.65 (3H, s) 2.59 (2H, m) 2.30 (2H, m) 2.0–1.8 (4H, m) 1.12 (3H, s).

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29
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- 3N: C 71.55 H 6.71 N 4.91, found C 71.53 H 6.44 N 4.89.

30
- 84918608963
- D. Desmaele, J. d'Angelo, Tetrahedron Lett., this Issue, following paper.

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